Benzyl-4-O-<6-O-acetyl-3-O-(3,4,6-tri-O-acetyl-2-desoxy-2-phthalimido-β-D-glucopyranosyl)-2,4-di-O-benzyl-β-D-galactopyranosyl>-2,3-O-isopropyliden-α-L-rhamnopyranosid

Base Information

Chemical Name:Benzyl-4-O-<6-O-acetyl-3-O-(3,4,6-tri-O-acetyl-2-desoxy-2-phthalimido-β-D-glucopyranosyl)-2,4-di-O-benzyl-β-D-galactopyranosyl>-2,3-O-isopropyliden-α-L-rhamnopyranosid
CAS No.:79705-62-7
Molecular Formula:C₅₈H₆₅NO₂₀
Molecular Weight:1096.15
Hs Code.:

Benzyl-4-O-<6-O-acetyl-3-O-(3,4,6-tri-O-acetyl-2-desoxy-2-phthalimido-β-D-glucopyranosyl)-2,4-di-O-benzyl-β-D-galactopyranosyl>-2,3-O-isopropyliden-α-L-rhamnopyranosid

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Chemical Property of Benzyl-4-O-<6-O-acetyl-3-O-(3,4,6-tri-O-acetyl-2-desoxy-2-phthalimido-β-D-glucopyranosyl)-2,4-di-O-benzyl-β-D-galactopyranosyl>-2,3-O-isopropyliden-α-L-rhamnopyranosid

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Technology Process of Benzyl-4-O-<6-O-acetyl-3-O-(3,4,6-tri-O-acetyl-2-desoxy-2-phthalimido-β-D-glucopyranosyl)-2,4-di-O-benzyl-β-D-galactopyranosyl>-2,3-O-isopropyliden-α-L-rhamnopyranosid

There total 2 articles about Benzyl-4-O-<6-O-acetyl-3-O-(3,4,6-tri-O-acetyl-2-desoxy-2-phthalimido-β-D-glucopyranosyl)-2,4-di-O-benzyl-β-D-galactopyranosyl>-2,3-O-isopropyliden-α-L-rhamnopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79705-54-7,79705-55-8,81661-81-6
1,6-Di-O-acetyl-2,4-di-O-benzyl-3-O-(3,4,6-tri-O-acetyl-2-desoxy-2-phthalimido-β-D-glucopyranosyl)-D-galactopyranose

: 79705-62-7
Benzyl-4-O-<6-O-acetyl-3-O-(3,4,6-tri-O-acetyl-2-desoxy-2-phthalimido-β-D-glucopyranosyl)-2,4-di-O-benzyl-β-D-galactopyranosyl>-2,3-O-isopropyliden-α-L-rhamnopyranosid

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / TiBr₄ / ethyl acetate; CH₂Cl₂ / 2 h / 0 °C

2: 1) Hg(CN)2, Hg(Br)2, molecular sieves 4 Angstroem / 1.) CH₂Cl₂, 1 h, r.t.; 2.) 0 deg C, CH₂Cl₂, 5 h

With 4 A molecular sieve; mercury(II) cyanide; titanium(IV) bromide; mercury dibromide; In dichloromethane; ethyl acetate;

Reference yield:

: 53270-14-7
benzyl 2,3-O-isopropylidene-α-L-rhamnopyranoside

: 79705-59-2
6-O-Acetyl-3-O-(3,4,6-tri-O-acetyl-2-desoxy-2-phthalimido-β-D-glucopyranosyl)-2,4-di-O-benzyl-α-D-galactopyranosylbromid

: 79705-62-7
Benzyl-4-O-<6-O-acetyl-3-O-(3,4,6-tri-O-acetyl-2-desoxy-2-phthalimido-β-D-glucopyranosyl)-2,4-di-O-benzyl-β-D-galactopyranosyl>-2,3-O-isopropyliden-α-L-rhamnopyranosid

: 79705-61-6
Benzyl-4-O-<6-O-acetyl-3-O-(3,4,6-tri-O-acetyl-2-desoxy-2-phthalimido-β-D-glucopyranosyl)-2,4-di-O-benzyl-α-D-galactopyranosyl>-2,3-O-isopropyliden-α-L-rhamnopyranosid

Guidance literature:: With 4 A molecular sieve; mercury(II) cyanide; mercury dibromide; Yield given. Multistep reaction. Yields of byproduct given; 1.) CH₂Cl₂, 1 h, r.t.; 2.) 0 deg C, CH₂Cl₂, 5 h;