8-bromo-3-chloro-5-phenyl-7H-dibenzazepine

Base Information

Chemical Name:8-bromo-3-chloro-5-phenyl-7H-dibenzazepine
CAS No.:172976-11-3
Molecular Formula:C₂₀H₁₃BrClN
Molecular Weight:382.687
Hs Code.:

8-bromo-3-chloro-5-phenyl-7H-dibenz<c,e>azepine

Synonyms:

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Chemical Property of 8-bromo-3-chloro-5-phenyl-7H-dibenzazepine

Chemical Property:

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Technology Process of 8-bromo-3-chloro-5-phenyl-7H-dibenzazepine

There total 9 articles about 8-bromo-3-chloro-5-phenyl-7H-dibenzazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-bromo-6-nitrotoluene: 55289-35-5
2-bromo-6-nitrotoluene

: 172976-11-3
8-bromo-3-chloro-5-phenyl-7H-dibenzazepine

Guidance literature:: Multi-step reaction with 8 steps

1: 1.) tetrakis(triphenylphosphine)palladium⁽⁰⁾, 2.) sodium carbonate / 1.) 1,2-dimethoxyethane, 20 min, 2.) 1,2-dimethoxyethane, water, reflux

2: 97 percent / hydrogen / Pd/C / ethanol

4: 87 percent / N-bromosuccinimide, benzoyl peroxide / CCl₄ / 1 h / Heating

5: 77 percent / dimethylformamide / Ambient temperature

6: 100 percent / hydrazine hydrate / methanol / Heating

7: 75 percent / sodium carbonate / CH₂Cl₂ / Ambient temperature

8: 1.) thionyl chloride, 2.) potassium tert-butoxide / 1.) ether, reflux, 2.) THF, 0 -> 20 deg C

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; thionyl chloride; Perbenzoic acid; potassium tert-butylate; hydrogen; sodium carbonate; hydrazine hydrate; palladium on activated charcoal; In methanol; tetrachloromethane; ethanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 603-83-8
3-nitro-o-tolylamine

: 172976-11-3
8-bromo-3-chloro-5-phenyl-7H-dibenzazepine

Guidance literature:: Multi-step reaction with 9 steps

1: 1.) NaNO₂, HBr, 2.) CuBr

2: 1.) tetrakis(triphenylphosphine)palladium⁽⁰⁾, 2.) sodium carbonate / 1.) 1,2-dimethoxyethane, 20 min, 2.) 1,2-dimethoxyethane, water, reflux

3: 97 percent / hydrogen / Pd/C / ethanol

5: 87 percent / N-bromosuccinimide, benzoyl peroxide / CCl₄ / 1 h / Heating

6: 77 percent / dimethylformamide / Ambient temperature

7: 100 percent / hydrazine hydrate / methanol / Heating

8: 75 percent / sodium carbonate / CH₂Cl₂ / Ambient temperature

9: 1.) thionyl chloride, 2.) potassium tert-butoxide / 1.) ether, reflux, 2.) THF, 0 -> 20 deg C

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; thionyl chloride; Perbenzoic acid; potassium tert-butylate; hydrogen bromide; hydrogen; sodium carbonate; hydrazine hydrate; copper(I) bromide; sodium nitrite; palladium on activated charcoal; In methanol; tetrachloromethane; ethanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 172975-97-2
2-(4-chlorophenyl)-6-nitrotoluene

: 172976-11-3
8-bromo-3-chloro-5-phenyl-7H-dibenzazepine

Guidance literature:: Multi-step reaction with 7 steps

1: 97 percent / hydrogen / Pd/C / ethanol

3: 87 percent / N-bromosuccinimide, benzoyl peroxide / CCl₄ / 1 h / Heating

4: 77 percent / dimethylformamide / Ambient temperature

5: 100 percent / hydrazine hydrate / methanol / Heating

6: 75 percent / sodium carbonate / CH₂Cl₂ / Ambient temperature

7: 1.) thionyl chloride, 2.) potassium tert-butoxide / 1.) ether, reflux, 2.) THF, 0 -> 20 deg C

With N-Bromosuccinimide; thionyl chloride; Perbenzoic acid; potassium tert-butylate; hydrogen; sodium carbonate; hydrazine hydrate; palladium on activated charcoal; In methanol; tetrachloromethane; ethanol; dichloromethane; N,N-dimethyl-formamide;