Technology Process of Cyclohexane, 1,1-dibromo-4-(1,1-dimethylethyl)-
There total 3 articles about Cyclohexane, 1,1-dibromo-4-(1,1-dimethylethyl)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
boron tribromide;
In
dichloromethane;
at 0 ℃;
for 8h;
DOI:10.1055/s-1986-31492
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 2.) p-toluenesulfonic acid / 1.) benzene, reflux, 2.) benzene, reflux
2: 82 percent / BBr3 / CH2Cl2 / 8 h / 0 °C
With
boron tribromide;
toluene-4-sulfonic acid;
In
dichloromethane;
DOI:10.1055/s-1986-31492
- Guidance literature:
-
Multi-step reaction with 3 steps
1: p-toluenesulfonic acid / methanol / Heating
2: 2.) p-toluenesulfonic acid / 1.) benzene, reflux, 2.) benzene, reflux
3: 82 percent / BBr3 / CH2Cl2 / 8 h / 0 °C
With
boron tribromide; toluene-4-sulfonic acid;
toluene-4-sulfonic acid;
In
methanol; dichloromethane;
DOI:10.1055/s-1986-31492
