(R)-3-(2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(4-((1-cyclopentenyl)ethynyl)phenyl)propanamido)propanoic acid(S)-3-(2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(4-(3-phenylprop-1-ynyl)phenyl)propanamido)propanoic acid

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Chemical Name:(R)-3-(2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(4-((1-cyclopentenyl)ethynyl)phenyl)propanamido)propanoic acid(S)-3-(2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(4-(3-phenylprop-1-ynyl)phenyl)propanamido)propanoic acid
CAS No.:1393723-85-7
Molecular Formula:C₃₄H₃₂N₂O₅
Molecular Weight:548.638
Hs Code.:

(R)-3-(2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(4-((1-cyclopentenyl)ethynyl)phenyl)propanamido)propanoic acid(S)-3-(2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(4-(3-phenylprop-1-ynyl)phenyl)propanamido)propanoic acid

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Chemical Property of (R)-3-(2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(4-((1-cyclopentenyl)ethynyl)phenyl)propanamido)propanoic acid(S)-3-(2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(4-(3-phenylprop-1-ynyl)phenyl)propanamido)propanoic acid

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Technology Process of (R)-3-(2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(4-((1-cyclopentenyl)ethynyl)phenyl)propanamido)propanoic acid(S)-3-(2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(4-(3-phenylprop-1-ynyl)phenyl)propanamido)propanoic acid

There total 1 articles about (R)-3-(2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(4-((1-cyclopentenyl)ethynyl)phenyl)propanamido)propanoic acid(S)-3-(2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(4-(3-phenylprop-1-ynyl)phenyl)propanamido)propanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1610-13-5
ethynylcyclopentene

: H-β-Ala-2-ClTrt resin

: 205526-29-0
(R)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(4-iodophenyl)propanoic acid

: 1393723-85-7
(R)-3-(2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(4-((1-cyclopentenyl)ethynyl)phenyl)propanamido)propanoic acid(S)-3-(2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(4-(3-phenylprop-1-ynyl)phenyl)propanamido)propanoic acid

Guidance literature:: H-β-Ala-2-ClTrt resin; (R)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-(4-iodophenyl)propanoic acid; With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 25 ℃; solid phase reaction;

ethynylcyclopentene; With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In 1,4-dioxane; at 25 ℃; Inert atmosphere; Darkness; solid phase reaction;

With trifluoroacetic acid; In dichloromethane; at 25 ℃; for 1h; solid phase reaction;
DOI:10.1002/chem.201200952