(diphenylphosphino)(diphenylstibino)methane

Base Information

Chemical Name:(diphenylphosphino)(diphenylstibino)methane
CAS No.:85472-42-0
Molecular Formula:C₂₅H₂₂PSb
Molecular Weight:475.173
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (diphenylphosphino)(diphenylstibino)methane

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Technology Process of (diphenylphosphino)(diphenylstibino)methane

There total 1 articles about (diphenylphosphino)(diphenylstibino)methane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 70080-28-3
{(diphenylstibino)methyl}lithium

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 85472-42-0
(diphenylphosphino)(diphenylstibino)methane

Guidance literature:: With water; In tetrahydrofuran; soln. warmed from -30°C to room temp., stirred for 2 h, hydrolysis; chloroform added, washed with water, dried above Na2SO4, solvent distd., remaining oil chromd., elem. anal.;

Reference yield: 31.0%

: 58751-37-4
pentacarbonyl(dimethyloxosulfoniomethanide)chromium

: 85472-42-0
(diphenylphosphino)(diphenylstibino)methane

: 101136-59-8
tetracarbonyl(diphenylstibinomethyl-diphenylphosphoniomethanide α-C, ω-Sb)chromium(0)

Guidance literature:: In toluene; (N2), mixture of Cr-complex and Sb-compound in toluene stirred at 45°C for 20 h; filtered, filtrate dried in vac., residue dissolved in CH2Cl2, petroleum ether added, filtered, washed with petroleum ether, dried; elem. anal.;