ethyl 6-O-acetyl-2,3,4-trideoxy-4--α-D-erythro-hex-2-enopyranoside

Base Information

Chemical Name:ethyl 6-O-acetyl-2,3,4-trideoxy-4--α-D-erythro-hex-2-enopyranoside
CAS No.:78081-22-8
Molecular Formula:C₁₉H₂₄O₈S
Molecular Weight:412.461
Hs Code.:

ethyl 6-O-acetyl-2,3,4-trideoxy-4-<methoxycarbonyl-(phenylsulfonyl)methyl>-α-D-erythro-hex-2-enopyranoside

Synonyms:

Suppliers and Price of ethyl 6-O-acetyl-2,3,4-trideoxy-4--α-D-erythro-hex-2-enopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 6-O-acetyl-2,3,4-trideoxy-4--α-D-erythro-hex-2-enopyranoside

Chemical Property:

Purity/Quality:

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Technology Process of ethyl 6-O-acetyl-2,3,4-trideoxy-4--α-D-erythro-hex-2-enopyranoside

There total 3 articles about ethyl 6-O-acetyl-2,3,4-trideoxy-4--α-D-erythro-hex-2-enopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 34097-60-4
methyl benzenesulfonylacetate

: 3323-72-6
ethyl 4,6-di-O-acetyl-2,3-dideoxy-α-D-erythrohex-2-enopyranoside

: 78081-22-8,78148-08-0
ethyl 6-O-acetyl-2,3,4-trideoxy-4--α-D-erythro-hex-2-enopyranoside

Guidance literature:: With sodium hydride; triphenylphosphine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; Heating; 1.) 48 h.; 2.) 24 h.;

Reference yield:

: 69055-68-1,3323-72-6,56196-39-5,61826-47-9,63976-48-7,78148-04-6
ethyl 4,6-di-O-acetyl-2,3-dideoxy-α-D-threo-hex-2-enopyranoside

: 34097-60-4
methyl benzenesulfonylacetate

: 78081-27-3
ethyl 6-O-acetyl-2,3,4-trideoxy-2--α-D-hex-3-enopyranoside

: 78081-22-8,78148-08-0
ethyl 6-O-acetyl-2,3,4-trideoxy-4--α-D-hex-2-enopyranoside

Guidance literature:: With sodium hydride; triphenylphosphine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; for 120h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Heating;

Reference yield:

: 52471-76-8,23339-15-3,56196-33-9,63526-95-4
ethyl 2,3-dideoxy-α-D-threo-hex-2-enopyranoside

: 78081-22-8,78148-08-0
ethyl 6-O-acetyl-2,3,4-trideoxy-4--α-D-hex-2-enopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 1 h / 25 °C

2: NaH, triphenylphosphine / tetrakis(triphenylphosphine)palladium⁽⁰⁾ / tetrahydrofuran / 120 h / Heating

With sodium hydride; triphenylphosphine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; pyridine;