[(3,5-bis(trifluoromethyl)-1H-pyrazolate-1-yl)-triphenylphosphane-gold(I)]

Base Information

Chemical Name:[(3,5-bis(trifluoromethyl)-1H-pyrazolate-1-yl)-triphenylphosphane-gold(I)]
CAS No.:85655-40-9
Molecular Formula:C₂₃H₁₆AuF₆N₂P
Molecular Weight:662.324
Hs Code.:

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Chemical Property of [(3,5-bis(trifluoromethyl)-1H-pyrazolate-1-yl)-triphenylphosphane-gold(I)]

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Technology Process of [(3,5-bis(trifluoromethyl)-1H-pyrazolate-1-yl)-triphenylphosphane-gold(I)]

There total 2 articles about [(3,5-bis(trifluoromethyl)-1H-pyrazolate-1-yl)-triphenylphosphane-gold(I)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 67215-70-7
(triphenylphosphine)gold(I) tetrafluoroborate

: 14704-41-7
3,5-bis(trifluoromethyl)pyrazole

: 85655-40-9
[(3,5-bis(trifluoromethyl)-1H-pyrazolate-1-yl)-triphenylphosphane-gold(I)]

Guidance literature:: With KOH; In tetrahydrofuran; methanol; to soln. 3,5-bis(trifluoromethyl)pyrazole in MeOH soln. KOH in MeOH was added, soln. Au complex in THF was added, stirred for 1 h; soln. was filtered and concd. to dryness in vacuo, residue was washed with hexane and crystd. from CH2Cl2-hexane; elem. anal.;
DOI:10.1039/c2dt11781a

Reference yield:

: 14243-64-2
(triphenylphosphine)gold(I) chloride

: 14704-41-7
3,5-bis(trifluoromethyl)pyrazole

: 85655-40-9
[(3,5-bis(trifluoromethyl)-1H-pyrazolate-1-yl)-triphenylphosphane-gold(I)]

Guidance literature:: With potassium hydroxide; In methanol; byproducts: Cl(1-); org. compd. and KOH (soln. in MeOH) added to a stirred suspn. of the Au-complex in MeOH; evapd., extd. with benzene, evapd. to dryness, dissolved in n-hexane, cooled to -15°C, elem. anal.;