C₁₇H₁₅NO₃

Base Information

Chemical Name:C₁₇H₁₅NO₃
CAS No.:1337936-07-8
Molecular Formula:C₁₇H₁₅NO₃
Molecular Weight:281.311
Hs Code.:

C<sub>17</sub>H<sub>15</sub>NO<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₇H₁₅NO₃

Chemical Property:

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Technology Process of C₁₇H₁₅NO₃

There total 5 articles about C₁₇H₁₅NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 1337936-06-7
C₁₈H₁₇NO₃

: 1337936-07-8
C₁₇H₁₅NO₃

Guidance literature:: With boron tribromide; In dichloromethane; at -78 - 20 ℃; for 24h; Inert atmosphere;
DOI:10.1021/jm2005404

Reference yield:

: 673-22-3
2-Hydroxy-4-methoxybenzaldehyde

: 1337936-07-8
C₁₇H₁₅NO₃

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / dichloromethane / 1 h / 20 °C

2: bromine; acetic acid / 1 h / 20 °C

3: 18-crown-6 ether; bis-(2,2,2-trifluoroethyl)(methoxycarbonylmethyl)phosphonate; potassium hexamethylsilazane / tetrahydrofuran; toluene / 4 h / -78 - 20 °C / Inert atmosphere

4: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; cesium fluoride / N,N-dimethyl-formamide / 3 h / 60 °C / Inert atmosphere

5: boron tribromide / dichloromethane / 24 h / -78 - 20 °C / Inert atmosphere

With pyridine; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; 18-crown-6 ether; bromine; bis-(2,2,2-trifluoroethyl)(methoxycarbonylmethyl)phosphonate; boron tribromide; potassium hexamethylsilazane; acetic acid; cesium fluoride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; 3: Horner-Wadsworth-Emmons olefination / 4: Suzuki-Miyaura cross-coupling reaction;
DOI:10.1021/jm2005404

Reference yield:

: 62536-84-9
2-formyl-5-methoxyphenyl acetate

: 1337936-07-8
C₁₇H₁₅NO₃

Guidance literature:: Multi-step reaction with 4 steps

1: bromine; acetic acid / 1 h / 20 °C

2: 18-crown-6 ether; bis-(2,2,2-trifluoroethyl)(methoxycarbonylmethyl)phosphonate; potassium hexamethylsilazane / tetrahydrofuran; toluene / 4 h / -78 - 20 °C / Inert atmosphere

3: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; cesium fluoride / N,N-dimethyl-formamide / 3 h / 60 °C / Inert atmosphere

4: boron tribromide / dichloromethane / 24 h / -78 - 20 °C / Inert atmosphere

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; 18-crown-6 ether; bromine; bis-(2,2,2-trifluoroethyl)(methoxycarbonylmethyl)phosphonate; boron tribromide; potassium hexamethylsilazane; acetic acid; cesium fluoride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; 2: Horner-Wadsworth-Emmons olefination / 3: Suzuki-Miyaura cross-coupling reaction;
DOI:10.1021/jm2005404