Technology Process of methyl 4-((dimethylcarbamoyl)oxy)-3-hydroxybenzoate
There total 2 articles about methyl 4-((dimethylcarbamoyl)oxy)-3-hydroxybenzoate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dipotassium peroxodisulfate; [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2; trifluoroacetic acid; trifluoroacetic anhydride;
at 80 ℃;
for 3h;
regioselective reaction;
Sealed tube;
DOI:10.1002/adsc.201300999
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate / acetonitrile / Sealed tube; Reflux
2: [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2; trifluoroacetic acid; dipotassium peroxodisulfate; trifluoroacetic anhydride / 3 h / 80 °C / Sealed tube
With
dipotassium peroxodisulfate; [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2; potassium carbonate; trifluoroacetic acid; trifluoroacetic anhydride;
In
acetonitrile;
DOI:10.1002/adsc.201300999
