N,N'-di-p-tolyl-N-ferrocenoylurea

Base Information

• Chemical Name: N,N'-di-p-tolyl-N-ferrocenoylurea
• CAS No.: 711027-48-4
• Molecular Formula: C₂₆H₂₄FeN₂O₂
• Molecular Weight: 452.336
• Mol file: 711027-48-4.mol

Synonyms:

Chemical Property of N,N'-di-p-tolyl-N-ferrocenoylurea

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of N,N'-di-p-tolyl-N-ferrocenoylurea

There total 1 articles about N,N'-di-p-tolyl-N-ferrocenoylurea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

ferrocenecarboxylic acid (1271-42-7) + di-p-tolylcarbodiimide (726-42-1) → ferrocenecarboxylic acid anhydride + N,N'-di-p-tolyl-N-ferrocenoylurea (711027-48-4)

Guidance literature:

In dichloromethane; Sonication; under Ar; Fe complex and carbodiimide (molar ratio 1:1.25) suspended in CH2Cl2 by means of ultrasonic bath; stirred at room temp. for 24 h; concd.; sepd. by column chromy. (silica gel, acetone-CH2Cl2); anhydride was in first fraction; second fraction collected; solvent removed by vac.; solid kept at 30°C and 0.1 mbar for 20 h; elem. anal.;

DOI:10.1016/j.jorganchem.2003.12.045

upstream raw materials:

ferrocenecarboxylic acid

di-p-tolylcarbodiimide