bis(mesitylphosphino)tris(trimethylsilyl)methylborane

Base Information

• Chemical Name: bis(mesitylphosphino)tris(trimethylsilyl)methylborane
• CAS No.: 1007126-61-5
• Molecular Formula: C₂₈H₅₁BP₂Si₃
• Molecular Weight: 544.728
• Mol file: 1007126-61-5.mol

Synonyms:

Chemical Property of bis(mesitylphosphino)tris(trimethylsilyl)methylborane

Chemical Property:

Purity/Quality:

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Technology Process of bis(mesitylphosphino)tris(trimethylsilyl)methylborane

There total 1 articles about bis(mesitylphosphino)tris(trimethylsilyl)methylborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

dichloro{tris(trimethylsilyl)methyl}borane (124408-70-4) + lithium 2,4,6-trimethylphenylhydrophosphanide (89634-37-7,147285-62-9) → bis(mesitylphosphino)tris(trimethylsilyl)methylborane (1007126-61-5)

Guidance literature:

In hexane; byproducts: LiCl; under Ar or N2, 2 equiv. of Li-compd. was added in hexane to hexane soln. of B-compd., stirring overnight; soln. was filtered, after isolation crystn. was performed from a small amt. of hexane at -30 °C, elem. anal.;

DOI:10.1002/zaac.200600335

upstream raw materials:

dichloro{tris(trimethylsilyl)methyl}borane

lithium 2,4,6-trimethylphenylhydrophosphanide