[HgCl2(μ-Cl)2(Te(Ph)CH2SiMe3)2]

Base Information

• Chemical Name: [HgCl2(μ-Cl)2(Te(Ph)CH2SiMe3)2]
• CAS No.: 1190293-71-0
• Molecular Formula: C₂₀H₃₂Cl₄Hg₂Si₂Te₂
• Molecular Weight: 1126.84

Synonyms:

Chemical Property of [HgCl2(μ-Cl)2(Te(Ph)CH2SiMe3)2]

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of [HgCl2(μ-Cl)2(Te(Ph)CH2SiMe3)2]

There total 3 articles about [HgCl2(μ-Cl)2(Te(Ph)CH2SiMe3)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.7%

phenyl(trimethylsilylmethyl)tellane (90304-55-5) + mercury dichloride → [HgCl2(Te(Ph)CH2SiMe3)2] (1190293-68-5) + [HgCl2(μ-Cl)2(Te(Ph)CH2SiMe3)2] (1190293-71-0)

Guidance literature:

In ethanol; dichloromethane; (Ar); tellurium compound (3 equiv.) was added to soln. of HgCl2 (1 equiv.), stirred for 15 min at room temp., evapd., CH2Cl2 was added, allowed to stand at room temp. for few minuts; evapd., hexane was added, filtered, filtrate was evapd., crystd. from CH2Cl2, elem. anal.;

DOI:10.1016/j.jorganchem.2009.05.021

Reference yield:

phenyl(trimethylsilylmethyl)tellane (90304-55-5) → [HgCl2(μ-Cl)2(Te(Ph)CH2SiMe3)2] (1190293-71-0)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol; dichloromethane

2: dichloromethane

In ethanol; dichloromethane;

DOI:10.1016/j.jorganchem.2009.05.021

Reference yield:

[HgCl2(Te(Ph)CH2SiMe3)2] (1190293-68-5) → [HgCl2(μ-Cl)2(Te(Ph)CH2SiMe3)2] (1190293-71-0)

Guidance literature:

In dichloromethane; byproducts: Te(C6H5)CH2Si(CH3)3;

DOI:10.1016/j.jorganchem.2009.05.021

upstream raw materials:

phenyl(trimethylsilylmethyl)tellane

[HgCl₂(Te(Ph)CH₂SiMe₃)2]

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