(1Z,3Z)-2,2-Dichloro-N~1~,N~3~-bis(4-methoxyphenyl)propanebis(imidoyl) dichloride

Base Information

• Chemical Name: (1Z,3Z)-2,2-Dichloro-N~1~,N~3~-bis(4-methoxyphenyl)propanebis(imidoyl) dichloride
• CAS No.: 105678-73-7
• Molecular Formula: C17H14Cl4N2O2
• Molecular Weight: 420.122
• DSSTox Substance ID: DTXSID80543364
• Mol file: 105678-73-7.mol

Synonyms:105678-73-7;DTXSID80543364;(1Z,3Z)-2,2-Dichloro-N~1~,N~3~-bis(4-methoxyphenyl)propanebis(imidoyl) dichloride

Chemical Property of (1Z,3Z)-2,2-Dichloro-N~1~,N~3~-bis(4-methoxyphenyl)propanebis(imidoyl) dichloride

Chemical Property:

• XLogP3: 6.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 6
• Exact Mass: 419.977988
• Heavy Atom Count: 25
• Complexity: 441

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=CC=C(C=C1)N=C(C(C(=NC2=CC=C(C=C2)OC)Cl)(Cl)Cl)Cl

Technology Process of (1Z,3Z)-2,2-Dichloro-N~1~,N~3~-bis(4-methoxyphenyl)propanebis(imidoyl) dichloride

There total 1 articles about (1Z,3Z)-2,2-Dichloro-N~1~,N~3~-bis(4-methoxyphenyl)propanebis(imidoyl) dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

N,N'-bis(4-methoxyphenyl)malonamide (15589-58-9) → 2,2-Dichloro-N1,N3-bis-(4-methoxy-phenyl)-propanediimidoyl dichloride (105678-73-7)

Guidance literature:

With phosphorus pentachloride; In toluene; for 5h; Heating;

Reference yield: 98.0%

2,2-Dichloro-N1,N3-bis-(4-methoxy-phenyl)-propanediimidoyl dichloride (105678-73-7) + triphenylphosphine (603-35-0) → [3-Chloro-6-methoxy-4-(4-methoxy-phenylamino)-quinolin-2-yl]-triphenyl-phosphonium; perchlorate

Guidance literature:

With sodium perchlorate; In benzene; at 20 ℃; for 24h;

Reference yield: 97.0%

2,2-Dichloro-N1,N3-bis-(4-methoxy-phenyl)-propanediimidoyl dichloride (105678-73-7) → bis<1-(p-methoxyphenyl)-5-tetrazolyl>dichloromethane (105678-79-3)

Guidance literature:

With sodium azide; In acetone; for 24h; Ambient temperature;

upstream raw materials:

N,N'-bis(4-methoxyphenyl)malonamide

Downstream raw materials:

N,N'-di(4-methoxyphenyl)dichloromalonamide

bis<1-(p-methoxyphenyl)-5-tetrazolyl>dichloromethane

4-(4-methoxyphenylamino)-6-methoxy-2,3-dichloroquinoline

5363780