Cl₂Ti(N(C₆H₄P(C₆H₅)2)(CH(C(CH₃)3)2))2

Base Information

• Chemical Name: Cl₂Ti(N(C₆H₄P(C₆H₅)2)(CH(C(CH₃)3)2))2
• CAS No.: 625458-42-6
• Molecular Formula: C₅₄H₆₆Cl₂N₂P₂Ti
• Molecular Weight: 923.865

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Chemical Property of Cl₂Ti(N(C₆H₄P(C₆H₅)2)(CH(C(CH₃)3)2))2

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Technology Process of Cl₂Ti(N(C₆H₄P(C₆H₅)2)(CH(C(CH₃)3)2))2

There total 1 articles about Cl₂Ti(N(C₆H₄P(C₆H₅)2)(CH(C(CH₃)3)2))2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

tetrachlorobis(tetrahydrofuran)titanium(IV) (31011-57-1,112925-19-6,112925-18-5) + (C6H5)2PC6H4N(Li)CH(C(CH3)3)2 → Cl2Ti(N(C6H4P(C6H5)2)(CH(C(CH3)3)2))2 (625458-42-6)

Guidance literature:

In toluene; Li salt and 0.5 equiv. of Ti complex in toluene soln.;

DOI:10.1021/om034164a

Reference yield: 85.0%

di(rhodium)tetracarbonyl dichloride + Cl2Ti(N(C6H4P(C6H5)2)(CH(C(CH3)3)2))2 (625458-42-6) → [TiCl2((C6H5)2PC6H4NCH(C(CH3)3)2)2RhCl(CO)]2

Guidance literature:

In dichloromethane; (N2); standard Schlenk technique; soln. of Ti complex in CH2Cl2 was added dropwise to soln. of Rh complex in CH2Cl2; mixt. was stirred at room temp. for 4 h; cooled to -20°C; elem. anal.;

DOI:10.1039/b402409e

Reference yield: 81.0%

bis(benzonitrile)palladium(II) dichloride (15617-18-2,39958-10-6,14220-64-5) + Cl2Ti(N(C6H4P(C6H5)2)(CH(C(CH3)3)2))2 (625458-42-6) → [TiCl2((C6H5)2PC6H4NCH(C(CH3)3)2)2PdCl2]

Guidance literature:

In toluene; (N2); standard Schlenk technique; soln. of Ti complex in toluene was added to stirred suspn. of Pd complex in toluene; soln. was stirred at roomtemp. for 8 h; solvent removed (vac.); redissolved in CH2Cl2; cooled to -20°C for 2 d; elem. anal.;

DOI:10.1039/b402409e

upstream raw materials:

tetrachlorobis(tetrahydrofuran)titanium(IV)

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