1-benzyloxy-2-(1'-hydroxyethyl)-4,5,6,8-tetramethoxy-3-prop-2''-enylnaphthalene

Base Information

Chemical Name:1-benzyloxy-2-(1'-hydroxyethyl)-4,5,6,8-tetramethoxy-3-prop-2''-enylnaphthalene
CAS No.:753009-23-3
Molecular Formula:C₂₆H₃₀O₆
Molecular Weight:438.521
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-benzyloxy-2-(1'-hydroxyethyl)-4,5,6,8-tetramethoxy-3-prop-2''-enylnaphthalene

Chemical Property:

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Technology Process of 1-benzyloxy-2-(1'-hydroxyethyl)-4,5,6,8-tetramethoxy-3-prop-2''-enylnaphthalene

There total 2 articles about 1-benzyloxy-2-(1'-hydroxyethyl)-4,5,6,8-tetramethoxy-3-prop-2''-enylnaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 753009-22-2
2-acetyl-1-benzyloxy-4,5,6,8-tetramethoxy-3-prop-2'-enylnaphthalene

: 753009-23-3
1-benzyloxy-2-(1'-hydroxyethyl)-4,5,6,8-tetramethoxy-3-prop-2''-enylnaphthalene

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 25 ℃; for 1h;
DOI:10.1055/s-2004-822370

Reference yield:

: 139269-54-8
2-acetyl-4-allyloxy-1-benzyloxy-5,6,8-trimethoxynaphthalene

: 753009-23-3
1-benzyloxy-2-(1'-hydroxyethyl)-4,5,6,8-tetramethoxy-3-prop-2''-enylnaphthalene

Guidance literature:: Multi-step reaction with 3 steps

1: 6 h / 160 °C

2: 213 mg / K₂CO₃ / acetone / 12 h / Heating

3: LiAlH₄ / diethyl ether / 1 h / 25 °C

With lithium aluminium tetrahydride; potassium carbonate; In diethyl ether; acetone; 1: Claisen rearrangement;
DOI:10.1055/s-2004-822370

Reference yield:

: 753009-23-3
1-benzyloxy-2-(1'-hydroxyethyl)-4,5,6,8-tetramethoxy-3-prop-2''-enylnaphthalene

: rac-(1R,3R)-10-benzyloxy-3,4-dihydro-5,6,7,9-tetramethoxy-1,3-dimethyl-1H-naphtho[2,3-c]pyran

: rac-(1R,3S)-10-benzyloxy-3,4-dihydro-5,6,7,9-tetramethoxy-1,3-dimethyl-1H-naphtho[2,3-c]pyran

Guidance literature:: 1-benzyloxy-2-(1'-hydroxyethyl)-4,5,6,8-tetramethoxy-3-prop-2''-enylnaphthalene; With mercury(II) diacetate; In tetrahydrofuran; for 1h;

With sodium hydroxide; sodium tetrahydroborate; In tetrahydrofuran; for 1h; Title compound not separated from byproducts;
DOI:10.1055/s-2004-822370