[Cu(I)(N,N'-(bis(pyridin-2-yl)C(Ph)-propane-1,3-diamine)]ClO₄

Base Information

• Chemical Name: [Cu(I)(N,N'-(bis(pyridin-2-yl)C(Ph)-propane-1,3-diamine)]ClO₄
• CAS No.: 866324-72-3
• Molecular Formula: C₂₇H₂₄CuN₄*ClO₄
• Molecular Weight: 567.511

Synonyms:

Chemical Property of [Cu(I)(N,N'-(bis(pyridin-2-yl)C(Ph)-propane-1,3-diamine)]ClO₄

Chemical Property:

Purity/Quality:

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Technology Process of [Cu(I)(N,N'-(bis(pyridin-2-yl)C(Ph)-propane-1,3-diamine)]ClO₄

There total 1 articles about [Cu(I)(N,N'-(bis(pyridin-2-yl)C(Ph)-propane-1,3-diamine)]ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

[Cu(N,N'-(bis(pyridin-2-yl)C(Ph)-propane-1,3-diamine)(N3)]ClO4 → [Cu(I)(N,N'-(bis(pyridin-2-yl)C(Ph)-propane-1,3-diamine)]ClO4 (866324-72-3)

Guidance literature:

With ascorbic acid; In methanol; water; aq. soln. of ascorbic acid added to suspn. of Cu compd. in MeOH with stirring, stirred for 30 min; filtered, washed with water and cold MeOH, dried in desiccator over CaCl2, chromy. (silica gel, CHCl3-MeOH (4:1), dried in air, crystals obtained by diffusion of CH2Cl2 soln. of complex to hexane layer; elem. anal.;

DOI:10.1016/j.poly.2005.04.023

Reference yield: 55.0%

sodium azide + [Cu(I)(N,N'-(bis(pyridin-2-yl)C(Ph)-propane-1,3-diamine)]ClO4 (866324-72-3) → [Cu(N,N'-(bis(pyridin-2-yl)C(Ph)-propane-1,3-diamine)(N3)]ClO4

Guidance literature:

With air; In methanol; water; aq. soln. of NaN3 added to suspn. of Cu compd. in MeOH, air passed through soln. for 30 min; filtered, kept in freezer for 4 h, filtered, washed with water and cold MeOH., compd. dissolved in mixt. of 2-methoxy-ethanol and MeOH (1:5), evapd. in air for 1 wk; elem. anal.;

DOI:10.1016/j.poly.2005.04.023

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