C₅₅H₈₃IO₆Si₂

Base Information

Chemical Name:C₅₅H₈₃IO₆Si₂
CAS No.:1435478-39-9
Molecular Formula:C₅₅H₈₃IO₆Si₂
Molecular Weight:1023.34
Hs Code.:

C<sub>55</sub>H<sub>83</sub>IO<sub>6</sub>Si<sub>2</sub>

Synonyms:

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Chemical Property of C₅₅H₈₃IO₆Si₂

Chemical Property:

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Technology Process of C₅₅H₈₃IO₆Si₂

There total 3 articles about C₅₅H₈₃IO₆Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1207069-42-8
C₂₁H₂₃IN₄O₄S

: 1435478-94-6
C₄₁H₆₆O₅Si₂

: 1435478-39-9
C₅₅H₈₃IO₆Si₂

: 1435478-96-8
C₅₅H₈₃IO₆Si₂

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; at -78 - 0 ℃; Overall yield = 88 %; Overall yield = 462 mg;
DOI:10.1039/c3ob40131f

Reference yield:

: 1435478-38-8
C₄₁H₆₈O₅Si₂

: 1435478-39-9
C₅₅H₈₃IO₆Si₂

: 1435478-96-8
C₅₅H₈₃IO₆Si₂

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 1 h / 0 °C

2: lithium hexamethyldisilazane / N,N,N,N,N,N-hexamethylphosphoric triamide; tetrahydrofuran / -78 - 0 °C

With sulfur trioxide pyridine complex; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; dimethyl sulfoxide;
DOI:10.1039/c3ob40131f

Reference yield:

: C₄₈H₇₄O₅Si₂

: 1435478-39-9
C₅₅H₈₃IO₆Si₂

: 1435478-96-8
C₅₅H₈₃IO₆Si₂

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen; 10 wt% Pd(OH)2 on carbon / methanol; ethyl acetate

2: triethylamine; sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 1 h / 0 °C

3: lithium hexamethyldisilazane / N,N,N,N,N,N-hexamethylphosphoric triamide; tetrahydrofuran / -78 - 0 °C

With 10 wt% Pd(OH)2 on carbon; hydrogen; sulfur trioxide pyridine complex; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; dimethyl sulfoxide; ethyl acetate;
DOI:10.1039/c3ob40131f