Fe(C₂₀H₈N₄(C₆H₅)3C₆H₄NHCOCHCHC₃H₃N₂)Cl

Base Information

• Chemical Name: Fe(C₂₀H₈N₄(C₆H₅)3C₆H₄NHCOCHCHC₃H₃N₂)Cl
• CAS No.: 91778-47-1
• Molecular Formula: C₅₀H₃₃ClFeN₇O
• Molecular Weight: 839.158
• Mol file: 91778-47-1.mol

Synonyms:

Chemical Property of Fe(C₂₀H₈N₄(C₆H₅)3C₆H₄NHCOCHCHC₃H₃N₂)Cl

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of Fe(C₂₀H₈N₄(C₆H₅)3C₆H₄NHCOCHCHC₃H₃N₂)Cl

There total 1 articles about Fe(C₂₀H₈N₄(C₆H₅)3C₆H₄NHCOCHCHC₃H₃N₂)Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C20H10N4(C6H5)3C6H4NHCOCHCHC3H3N2 + iron(II) chloride → Fe(C20H8N4(C6H5)3C6H4NHCOCHCHC3H3N2)Cl (91778-47-1)

Guidance literature:

In N,N-dimethyl-formamide; anhyd. FeCl2 was refluxed with ligand in DMF for 30 min in the dark; chromd. on silica gel column, recrystd. from toluene-hexane;

DOI:10.1039/c39840000359

Reference yield:

copper acetylacetonate + Fe(C20H8N4(C6H5)3C6H4NHCOCHCHC3H3N2)Cl (91778-47-1) → Fe(C20H8N4(C6H5)3C6H4NHCOCHCHC3H2N2)Cu(CH3COCHCOCH3)2

Guidance literature:

With potassium tert-butylate; In dichloromethane; soln. of Fe-complex, Cu(CH3COCHCOCH3)2 and t-BuOK (molar ratio 1:1.1:1)in CH2Cl2 was refluxed;

DOI:10.1039/c39840000359