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Re2Cl5(P(CH3)(C6H5)2)3(1+)*PF6(1-)=Re2Cl5(P(CH3)(C6H5)2)3PF6

Base Information
  • Chemical Name:Re2Cl5(P(CH3)(C6H5)2)3(1+)*PF6(1-)=Re2Cl5(P(CH3)(C6H5)2)3PF6
  • CAS No.:93806-29-2
  • Molecular Formula:C39H39Cl5P3Re2*F6P
  • Molecular Weight:1295.3
  • Hs Code.:
Re<sub>2</sub>Cl<sub>5</sub>(P(CH<sub>3</sub>)(C<sub>6</sub>H<sub>5</sub>)2)3<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=Re<sub>2</sub>Cl<sub>5</sub>(P(CH<sub>3</sub>)(C<sub>6</sub>H<sub>5</sub>)2)3PF<sub>6</sub>

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Chemical Property of Re2Cl5(P(CH3)(C6H5)2)3(1+)*PF6(1-)=Re2Cl5(P(CH3)(C6H5)2)3PF6
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Technology Process of Re2Cl5(P(CH3)(C6H5)2)3(1+)*PF6(1-)=Re2Cl5(P(CH3)(C6H5)2)3PF6

There total 1 articles about Re2Cl5(P(CH3)(C6H5)2)3(1+)*PF6(1-)=Re2Cl5(P(CH3)(C6H5)2)3PF6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In acetonitrile; Re-complex was suspended in acetonitrile, NOPF6 was added, KPF6 was added under N2, mixt. was chilled to 0°C;; filtered, washed with EtOH and Et2O, dried under reduced pressure; elem. anal.;;
Guidance literature:
In dichloromethane; byproducts: P(CH3)(C6H5)2, PF6(1-); Electrochem. Process; Cl(1-) was added to electrochem. cell containing Re-complex in n-Bu4NPF6-CH2Cl2;; not isolated, detected by cyclic voltammetry;;
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