[Ir(2-(coumaryl-6-azo)-4-phenyl-imidazole-H)(CO)(triphenylphosphine)2]

Base Information

Chemical Name:[Ir(2-(coumaryl-6-azo)-4-phenyl-imidazole-H)(CO)(triphenylphosphine)2]
CAS No.:1310359-50-2
Molecular Formula:C₅₅H₄₁IrN₄O₃P₂
Molecular Weight:1060.12
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Ir(2-(coumaryl-6-azo)-4-phenyl-imidazole-H)(CO)(triphenylphosphine)2]

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Technology Process of [Ir(2-(coumaryl-6-azo)-4-phenyl-imidazole-H)(CO)(triphenylphosphine)2]

There total 1 articles about [Ir(2-(coumaryl-6-azo)-4-phenyl-imidazole-H)(CO)(triphenylphosphine)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 15318-31-7,14871-41-1,59246-46-7
bis(triphenylphosphine)iridium(I) carbonyl chloride

: 1310359-47-7
2-(coumarin-6-ylazo)-4-phenyl-imidazole

: 1310359-50-2
[Ir(2-(coumaryl-6-azo)-4-phenyl-imidazole-H)(CO)(triphenylphosphine)2]

Guidance literature:: With Et₃N; In tetrahydrofuran; under N2; to a soln. of a ligand (0.21 mmol) in THF, NEt3 was added; stirring at room temp. for 15 min; Ir-contg. compd. (0.21 mmol) was added; stirring for 12 h; the solvent was removed under reduced pressure; the compd. was washed with H2O, Et2O and dried; column chromy. (alumina, benzene-acetonitrile (1:5 v/v) mixt.; diffusion of the CH2Cl2 soln. of the complex layered withhexane; elem. anal.;
DOI:10.1016/j.poly.2011.03.021