tri(carbonyl-κC)[meso-cis-2,6,10-triphenyl-2,6,10-triphospha-κ3P-bicyclo[9.4.0]pentadeca-11(1),12,14-triene]tungsten(O)

Base Information

Chemical Name:tri(carbonyl-κC)[meso-cis-2,6,10-triphenyl-2,6,10-triphospha-κ3P-bicyclo[9.4.0]pentadeca-11(1),12,14-triene]tungsten(O)
CAS No.:79190-85-5
Molecular Formula:C₃₃H₃₁O₃P₃W
Molecular Weight:752.379
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tri(carbonyl-κC)[meso-cis-2,6,10-triphenyl-2,6,10-triphospha-κ3P-bicyclo[9.4.0]pentadeca-11(1),12,14-triene]tungsten(O)

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Technology Process of tri(carbonyl-κC)[meso-cis-2,6,10-triphenyl-2,6,10-triphospha-κ3P-bicyclo[9.4.0]pentadeca-11(1),12,14-triene]tungsten(O)

There total 1 articles about tri(carbonyl-κC)[meso-cis-2,6,10-triphenyl-2,6,10-triphospha-κ3P-bicyclo[9.4.0]pentadeca-11(1),12,14-triene]tungsten(O) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 14040-11-0
tungsten hexacarbonyl

: 65113-29-3
2,6,10-triphenyl-2,6,10-triphosphabicyclo<9.4.0>pentadeca-11(1),12,14-triene

: 79190-85-5
tri(carbonyl-κC)[meso-cis-2,6,10-triphenyl-2,6,10-triphospha-κ3P-bicyclo[9.4.0]pentadeca-11(1),12,14-triene]tungsten(O)

Guidance literature:: In 1,3,5-trimethyl-benzene; heating mixt. of W(CO)6 and 1:1 mixt. of meso-cis and meso-trans ligandin degassed mesitylene at 165°C for 16 h; reaction was monitoredby IR spectroscopy;; filtered while hot; cooling to room temp.; crystn. of analytically pureproduct; elem. anal.;;