chloro-cis-bis{(2-methoxyethyl)phenyl(3-trimethoxysilylpropyl)phosphane-P;O',P'}palladium(II) hexafluoroantimonate

Base Information

Chemical Name:chloro-cis-bis{(2-methoxyethyl)phenyl(3-trimethoxysilylpropyl)phosphane-P;O',P'}palladium(II) hexafluoroantimonate
CAS No.:147282-03-9
Molecular Formula:C₃₀H₅₄ClO₈P₂PdSi₂*F₆Sb
Molecular Weight:1038.49
Hs Code.:

Synonyms:

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Chemical Property of chloro-cis-bis{(2-methoxyethyl)phenyl(3-trimethoxysilylpropyl)phosphane-P;O',P'}palladium(II) hexafluoroantimonate

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Technology Process of chloro-cis-bis{(2-methoxyethyl)phenyl(3-trimethoxysilylpropyl)phosphane-P;O',P'}palladium(II) hexafluoroantimonate

There total 4 articles about chloro-cis-bis{(2-methoxyethyl)phenyl(3-trimethoxysilylpropyl)phosphane-P;O',P'}palladium(II) hexafluoroantimonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 173142-52-4,147300-25-2
trans-dichlorobis{(2-methoxyethyl)phenyl(3-trimethoxypropyl)phosphane}palladium(II)

: 147282-03-9
trans-chlorobis{(2-methoxyethyl)phenyl(3-trimethoxysilylpropyl)phosphane-P;O',P'}palladium(II) hexafluoroantimonate

: 147282-03-9
chloro-cis-bis{(2-methoxyethyl)phenyl(3-trimethoxysilylpropyl)phosphane-P;O',P'}palladium(II) hexafluoroantimonate

Guidance literature:: With AgSbF₆; In tetrahydrofuran; byproducts: AgCl; dropwise addn. of AgSbF6 in THF to the Pd compd. in THF under Ar and in the dark and stirring for 2 h in the dark; filtn., evapn. (vac.), stirring of the residue in ether for 10 h, decantation and drying of the oil; elem. anal.;

Reference yield: 74.0%

: 173142-52-4,147300-25-2
trans-dichlorobis{(2-methoxyethyl)phenyl(3-trimethoxypropyl)phosphane}palladium(II)

: 147282-03-9
trans-chlorobis{(2-methoxyethyl)phenyl(3-trimethoxysilylpropyl)phosphane-P;O',P'}palladium(II) hexafluoroantimonate

: 147282-03-9
chloro-cis-bis{(2-methoxyethyl)phenyl(3-trimethoxysilylpropyl)phosphane-P;O',P'}palladium(II) hexafluoroantimonate

Guidance literature:: With AgSbF₆; In tetrahydrofuran; byproducts: AgCl; dropwise addn. of AgSbF6 in THF to the Pd compd. in THF under Ar and in the dark and stirring for 2 h in the dark; filtn., evapn. (vac.), stirring of the residue in ether for 10 h, decantation and drying of the oil; elem. anal.;

Reference yield:

: Si(OCH₃)3C₃H₆P(C₆H₅)CH₂OCH₃

: 147282-03-9
trans-chlorobis{(2-methoxyethyl)phenyl(3-trimethoxysilylpropyl)phosphane-P;O',P'}palladium(II) hexafluoroantimonate

: 147282-03-9
chloro-cis-bis{(2-methoxyethyl)phenyl(3-trimethoxysilylpropyl)phosphane-P;O',P'}palladium(II) hexafluoroantimonate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran

2: AgSbF₆ / tetrahydrofuran

With AgSbF₆; In tetrahydrofuran;