WI₂(CO)3(P(OC₆H₅)3)2*(C₂H₅)2O

Base Information

• Chemical Name: WI₂(CO)3(P(OC₆H₅)3)2*(C₂H₅)2O
• CAS No.: 214747-71-4
• Molecular Formula: C₄H₁₀O*C₃₉H₃₀I₂O₉P₂W
• Molecular Weight: 1216.39
• Mol file: 214747-71-4.mol

Synonyms:

Chemical Property of WI₂(CO)3(P(OC₆H₅)3)2*(C₂H₅)2O

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of WI₂(CO)3(P(OC₆H₅)3)2*(C₂H₅)2O

There total 1 articles about WI₂(CO)3(P(OC₆H₅)3)2*(C₂H₅)2O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

triphenyl phosphite (101-02-0) + bis(acetonitrile)diiodotricarbonyltungsten(II) (113350-36-0,102382-37-6) → WI2(CO)3(P(OC6H5)3)2*(C2H5)2O (214747-71-4)

Guidance literature:

In diethyl ether; N2-atmosphere; stirring W-complex with 2 equiv. of phosphite for 3 h; solvent removal (vac.), crystn. (-5°C, 72 h); elem. anal.;

DOI:10.1016/S0022-328X(98)00723-2

upstream raw materials:

triphenyl phosphite

bis(acetonitrile)diiodotricarbonyltungsten(II)