C₂₄H₃₈O₆Si

Base Information

Chemical Name:C₂₄H₃₈O₆Si
CAS No.:1388152-94-0
Molecular Formula:C₂₄H₃₈O₆Si
Molecular Weight:450.648
Hs Code.:

C<sub>24</sub>H<sub>38</sub>O<sub>6</sub>Si

Synonyms:

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Chemical Property of C₂₄H₃₈O₆Si

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Technology Process of C₂₄H₃₈O₆Si

There total 11 articles about C₂₄H₃₈O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₄H₃₈O₅Si

: C₂₄H₃₈O₆Si

: 1388152-94-0
C₂₄H₃₈O₆Si

Guidance literature:: C₂₄H₃₈O₅Si; With titanium(IV) isopropylate; (-)-diethyl tartrate; In dichloromethane; at -20 ℃; for 0.5h; Molecular sieve;

With tert.-butylhydroperoxide; In 2,2,4-trimethylpentane; dichloromethane; at -20 ℃; optical yield given as %de; Molecular sieve;
DOI:10.1021/ja305864z

Reference yield:

: C₂₇H₄₇BO₄Si

: 1388152-94-0
C₂₄H₃₈O₆Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; water / 2 h / 0 - 20 °C

2.1: 2,6-dimethylpyridine / dichloromethane / 0.5 h / 0 °C

3.1: camphor-10-sulfonic acid / methanol; dichloromethane / 5 h / 0 °C

4.1: sulfur trioxide pyridine complex; triethylamine / dichloromethane; dimethyl sulfoxide / 1 h / 0 °C

5.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C

5.2: 2 h / -78 - 0 °C

6.1: tetrahydrofuran / 0.5 h / 20 °C

7.1: dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; water / 2 h / 0 - 20 °C

8.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane / 1.5 h / 20 °C

8.2: 1 h / 20 °C

9.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.5 h / -78 °C / Inert atmosphere

10.1: titanium(IV) isopropylate; (-)-diethyl tartrate / dichloromethane / 0.5 h / -20 °C / Molecular sieve

10.2: -20 °C / Molecular sieve

With 2,6-dimethylpyridine; titanium(IV) isopropylate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; (-)-diethyl tartrate; camphor-10-sulfonic acid; potassium tert-butylate; dihydrogen peroxide; sulfur trioxide pyridine complex; diisobutylaluminium hydride; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; hexane; dichloromethane; water; dimethyl sulfoxide; 10.1: Sharpless epoxidation / 10.2: Sharpless epoxidation;
DOI:10.1021/ja305864z

Reference yield:

: 1388153-25-0
C₂₇H₄₈O₅Si₂

: 1388152-94-0
C₂₄H₃₈O₆Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: camphor-10-sulfonic acid / methanol; dichloromethane / 5 h / 0 °C

2.1: sulfur trioxide pyridine complex; triethylamine / dichloromethane; dimethyl sulfoxide / 1 h / 0 °C

3.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C

3.2: 2 h / -78 - 0 °C

4.1: tetrahydrofuran / 0.5 h / 20 °C

5.1: dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; water / 2 h / 0 - 20 °C

6.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane / 1.5 h / 20 °C

6.2: 1 h / 20 °C

7.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.5 h / -78 °C / Inert atmosphere

8.1: titanium(IV) isopropylate; (-)-diethyl tartrate / dichloromethane / 0.5 h / -20 °C / Molecular sieve

8.2: -20 °C / Molecular sieve

With titanium(IV) isopropylate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; (-)-diethyl tartrate; camphor-10-sulfonic acid; potassium tert-butylate; dihydrogen peroxide; sulfur trioxide pyridine complex; diisobutylaluminium hydride; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; hexane; dichloromethane; water; dimethyl sulfoxide; 8.1: Sharpless epoxidation / 8.2: Sharpless epoxidation;
DOI:10.1021/ja305864z