((t-Bu)3SiO)3TaCH₂

Base Information

Chemical Name:((t-Bu)3SiO)3TaCH₂
CAS No.:1242420-48-9
Molecular Formula:C₃₇H₈₃O₃Si₃Ta
Molecular Weight:841.269
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Chemical Property of ((t-Bu)3SiO)3TaCH₂

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Technology Process of ((t-Bu)3SiO)3TaCH₂

There total 1 articles about ((t-Bu)3SiO)3TaCH₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: 104092-13-9
(t-Bu₃SiO)3Ta

: 19493-09-5
Methylenetriphenylphosphorane

: 1242420-48-9
((t-Bu)3SiO)3TaCH₂

: 1242420-49-0
((t-Bu)3SiO)3TaCPPh₃

Guidance literature:: In tetrahydrofuran; byproducts: (C6H5)3P; Schlenk techniques; addn. of THF to Ta compd. and P compd. at -78°C, slow warming to 23°C over 12 h; degasification, filtration, concn., cooling to -78°C, filtration,dissolving filtrate in C5H12, cooling to -78°C, isolation of sol id, dissolving in C6H6, addn. of MeI, stirring overnight, filtration, evapn. in vacuo;
DOI:10.1021/ic101147x