1,2-bis(4-pyridyl)hexaphenylbenzene

Base Information

Chemical Name:1,2-bis(4-pyridyl)hexaphenylbenzene
CAS No.:1189377-78-3
Molecular Formula:C₅₂H₃₆N₂
Molecular Weight:688.871
Hs Code.:

Synonyms:

Suppliers and Price of 1,2-bis(4-pyridyl)hexaphenylbenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1,2-bis(4-pyridyl)hexaphenylbenzene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,2-bis(4-pyridyl)hexaphenylbenzene

There total 4 articles about 1,2-bis(4-pyridyl)hexaphenylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 1189377-77-2
1,2-bis(4-(pyridin-4-yl)phenyl)ethyne

: 479-33-4
2,3,4,5-tetraphenylcyclopenta-2,4-dienone

: 1189377-78-3
1,2-bis(4-pyridyl)hexaphenylbenzene

Guidance literature:: at 280 ℃; for 24h; Inert atmosphere;
DOI:10.1021/ja905796z

Reference yield: 22.0%

: 1189377-77-2
1,2-bis(4-(pyridin-4-yl)phenyl)ethyne

: 130567-71-4
tetraphenylcyclopentadienone

: 1189377-78-3
1,2-bis(4-pyridyl)hexaphenylbenzene

Guidance literature:: at 280 ℃; for 24h; Inert atmosphere;
DOI:10.1021/ja209254r

Reference yield:

: 5405-28-7
1,2-di(4-bromophenyl)-1,2-dibromoethane

: 1189377-78-3
1,2-bis(4-pyridyl)hexaphenylbenzene

Guidance literature:: Multi-step reaction with 3 steps

1: sodium ethanolate

2: bis-triphenylphosphine-palladium(II) chloride; sodium hydrogencarbonate

3: 24 h / 280 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; sodium ethanolate; sodium hydrogencarbonate; 2: Suzuki coupling / 3: Diels-Alder reaction;
DOI:10.1021/ja209254r