(((CH₃)3C₆H₂NSi(CH₃)2)2O)2Th

Base Information

• Chemical Name: (((CH₃)3C₆H₂NSi(CH₃)2)2O)2Th
• CAS No.: 866597-04-8
• Molecular Formula: C₄₄H₆₈N₄O₂Si₄Th
• Molecular Weight: 1029.43
• Mol file: 866597-04-8.mol

Synonyms:

Chemical Property of (((CH₃)3C₆H₂NSi(CH₃)2)2O)2Th

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of (((CH₃)3C₆H₂NSi(CH₃)2)2O)2Th

There total 1 articles about (((CH₃)3C₆H₂NSi(CH₃)2)2O)2Th which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

H2[(Mes)NON] (69981-85-7) + thorium tetrachloride (10026-08-1) → (((CH3)3C6H2NSi(CH3)2)2O)2Th (866597-04-8)

Guidance literature:

With n-BuLi; In diethyl ether; hexane; toluene; byproducts: LiCl; under N2; ligand dissolved in Et2O; soln. of n-BuLi (2 equiv.) in hexaneadded dropwise at -78°C; stirred at room temp. for 1 h; added dr opwise to toluene slurry of ThCl4 (0.5 equiv.); stirred for 15 h; filtered through Celite; solvent removed under reduced pressure; elem. anal.;

DOI:10.1039/b506180f

upstream raw materials:

H₂[(Mes)NON]

thorium tetrachloride