C₂₉H₄₆Cl₃N₃O₅Si

Base Information

Chemical Name:C₂₉H₄₆Cl₃N₃O₅Si
CAS No.:1313283-88-3
Molecular Formula:C₂₉H₄₆Cl₃N₃O₅Si
Molecular Weight:651.146
Hs Code.:

C<sub>29</sub>H<sub>46</sub>Cl<sub>3</sub>N<sub>3</sub>O<sub>5</sub>Si

Synonyms:

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Chemical Property of C₂₉H₄₆Cl₃N₃O₅Si

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Technology Process of C₂₉H₄₆Cl₃N₃O₅Si

There total 5 articles about C₂₉H₄₆Cl₃N₃O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1313289-06-3
C₂₁H₃₇Cl₃N₂O₆Si

: 64-04-0
phenethylamine

: 1313283-88-3
C₂₉H₄₆Cl₃N₃O₅Si

Guidance literature:: With 2,6-dimethylpyridine; 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 25 ℃;
DOI:10.1021/ja201878v

Reference yield:

: trans-4-(methoxycarbonyl)pyrrolidine-3-carboxylic acid

: 1313283-88-3
C₂₉H₄₆Cl₃N₃O₅Si

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydrogencarbonate; sodium carbonate / 1,4-dioxane; water / 0 °C / pH 9

2: 2,6-dimethylpyridine; 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 25 °C

3: lithium hydroxide monohydrate / water; tert-butyl alcohol / 0 °C

4: 2,6-dimethylpyridine; 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 25 °C

With 2,6-dimethylpyridine; 1-hydroxy-7-aza-benzotriazole; lithium hydroxide monohydrate; sodium hydrogencarbonate; sodium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In 1,4-dioxane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/ja201878v

Reference yield:

: C₁₀H₁₂Cl₃NO₆

: 1313283-88-3
C₂₉H₄₆Cl₃N₃O₅Si

Guidance literature:: Multi-step reaction with 3 steps

1: 2,6-dimethylpyridine; 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 25 °C

2: lithium hydroxide monohydrate / water; tert-butyl alcohol / 0 °C

3: 2,6-dimethylpyridine; 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 25 °C

With 2,6-dimethylpyridine; 1-hydroxy-7-aza-benzotriazole; lithium hydroxide monohydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/ja201878v