tricyclohexylphosphine-copper chloride

Base Information

Chemical Name:tricyclohexylphosphine-copper chloride
CAS No.:146056-09-9
Molecular Formula:C₁₈H₃₃ClCuP
Molecular Weight:379.433
Hs Code.:

Synonyms:

Suppliers and Price of tricyclohexylphosphine-copper chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of tricyclohexylphosphine-copper chloride

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of tricyclohexylphosphine-copper chloride

There total 1 articles about tricyclohexylphosphine-copper chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: sodium 2-[tert-butyl(phenyl)phosphanyl]phenolate

: Hoveyda-Grubbs catalyst first generation

: copper(l) chloride

: 2622-14-2
tricyclohexylphosphine

: [(OC₆H₄P(C₆H₅)C(CH₃)3)RuCl(HCC₆H₄OCH(CH₃)2)]

: 146056-09-9
Cu⁽¹⁺⁾*Cl^(1-)*P(C₆H₁₁)3=CuCl(P(C₆H₁₁)3)

: [(OC₆H₄P(C₆H₅)C(CH₃)3)2Ru(HCC₆H₄OCH(CH₃)2)]

: [(OC₆H₄P(C₆H₅)C(CH₃)3)2Ru(HCC₆H₄OCH(CH₃)2)]

Guidance literature:: In CD₂Cl₂; (Ar); std. Schlenk technique; Ru complex and PCy3 (8 equiv.) were mixed in CD2Cl2 in NMR tube; Na salt of ligand (0.8 equiv.) was added; CuCl was added; stirred for 30 min; NMR monitoring; not isolated;
DOI:10.1021/om100185g

Reference yield: 82.0%

: 146056-09-9
tricyclohexylphosphine-copper chloride

: 1118-67-8
sodium (Z)-4-oxopent-2-en-2-olate

: (CH₃COCHCOCH₃)CuP(C₆H₁₁)3

Guidance literature:: In pentane; byproducts: NaCl; nitrogen atmosphere; placing Cu-complex and org. compd. in Schlenk flask, pentane addn., stirring (2 h, room temp.); volatiles removal (vac.), crystn. on cooling pentane soln. at -30°C overnight; elem. anal.;

Reference yield: 75.0%

: 146056-09-9
tricyclohexylphosphine-copper chloride

: hexafluoroacetylacetone sodium salt

: (CF₃COCHCOCF₃)CuP(C₆H₁₁)3

Guidance literature:: In pentane; byproducts: NaCl; nitrogen atmosphere; placing Cu-complex and org. compd. in Schlenk flask, pentane addn., stirring (2 h, room temp.); volatiles removal (vac.), crystn. on cooling pentane soln. at -30°C overnight; elem. anal.;