{2-[Benzyloxycarbonyl-(6-{2-(3H-imidazol-4-yl)-1-[3-(3-{3-[3-(7-oxo-7H-furo[3,2-g]chromen-9-yloxy)-propylcarbamoyl]-propylcarbamoyl}-propylcarbamoyl)-propylcarbamoyl]-ethylcarbamoyl}-pyridin-2-ylmethyl)-amino]-ethyl}-carbamic acid benzyl ester

Base Information

• Chemical Name: {2-[Benzyloxycarbonyl-(6-{2-(3H-imidazol-4-yl)-1-[3-(3-{3-[3-(7-oxo-7H-furo[3,2-g]chromen-9-yloxy)-propylcarbamoyl]-propylcarbamoyl}-propylcarbamoyl)-propylcarbamoyl]-ethylcarbamoyl}-pyridin-2-ylmethyl)-amino]-ethyl}-carbamic acid benzyl ester
• CAS No.: 119829-32-2
• Molecular Formula: C₅₇H₆₄N₁₀O₁₃
• Molecular Weight: 1097.19

Synonyms:

Chemical Property of {2-[Benzyloxycarbonyl-(6-{2-(3H-imidazol-4-yl)-1-[3-(3-{3-[3-(7-oxo-7H-furo[3,2-g]chromen-9-yloxy)-propylcarbamoyl]-propylcarbamoyl}-propylcarbamoyl)-propylcarbamoyl]-ethylcarbamoyl}-pyridin-2-ylmethyl)-amino]-ethyl}-carbamic acid benzyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of {2-[Benzyloxycarbonyl-(6-{2-(3H-imidazol-4-yl)-1-[3-(3-{3-[3-(7-oxo-7H-furo[3,2-g]chromen-9-yloxy)-propylcarbamoyl]-propylcarbamoyl}-propylcarbamoyl)-propylcarbamoyl]-ethylcarbamoyl}-pyridin-2-ylmethyl)-amino]-ethyl}-carbamic acid benzyl ester

There total 9 articles about {2-[Benzyloxycarbonyl-(6-{2-(3H-imidazol-4-yl)-1-[3-(3-{3-[3-(7-oxo-7H-furo[3,2-g]chromen-9-yloxy)-propylcarbamoyl]-propylcarbamoyl}-propylcarbamoyl)-propylcarbamoyl]-ethylcarbamoyl}-pyridin-2-ylmethyl)-amino]-ethyl}-carbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

4-Amino-N-(3-{3-[3-(7-oxo-7H-furo[3,2-g]chromen-9-yloxy)-propylcarbamoyl]-propylcarbamoyl}-propyl)-butyramide (119829-31-1) + 2-[(6-{[Benzyloxycarbonyl-(2-benzyloxycarbonylamino-ethyl)-amino]-methyl}-pyridine-2-carbonyl)-amino]-3-(3H-imidazol-4-yl)-propionic acid (119802-78-7) → {2-[Benzyloxycarbonyl-(6-{2-(3H-imidazol-4-yl)-1-[3-(3-{3-[3-(7-oxo-7H-furo[3,2-g]chromen-9-yloxy)-propylcarbamoyl]-propylcarbamoyl}-propylcarbamoyl)-propylcarbamoyl]-ethylcarbamoyl}-pyridin-2-ylmethyl)-amino]-ethyl}-carbamic acid benzyl ester (119829-32-2)

Guidance literature:

With benzotriazol-1-ol; dicyclohexyl-carbodiimide;

DOI:10.1246/cl.1989.51

Reference yield:

8-hydroxypsoralen (2009-24-7) → {2-[Benzyloxycarbonyl-(6-{2-(3H-imidazol-4-yl)-1-[3-(3-{3-[3-(7-oxo-7H-furo[3,2-g]chromen-9-yloxy)-propylcarbamoyl]-propylcarbamoyl}-propylcarbamoyl)-propylcarbamoyl]-ethylcarbamoyl}-pyridin-2-ylmethyl)-amino]-ethyl}-carbamic acid benzyl ester (119829-32-2)

Guidance literature:

Multi-step reaction with 9 steps

1: 91 percent / K₂CO₃ / butan-2-one / 48 h / Heating

2: trifluoroacetic acid / CH₂Cl₂

3: 94 percent

4: trifluoroacetic acid / CH₂Cl₂

6: trifluoroacetic acid / CH₂Cl₂

8: trifluoroacetic acid / CH₂Cl₂

9: 40 percent / dicyclohexylcarbodiimide, 1-hydroxybenzotriazole

With potassium carbonate; benzotriazol-1-ol; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane; butanone;

DOI:10.1246/cl.1989.51

Reference yield:

9-(3-Amino-propoxy)-furo[3,2-g]chromen-7-one (119802-72-1) → {2-[Benzyloxycarbonyl-(6-{2-(3H-imidazol-4-yl)-1-[3-(3-{3-[3-(7-oxo-7H-furo[3,2-g]chromen-9-yloxy)-propylcarbamoyl]-propylcarbamoyl}-propylcarbamoyl)-propylcarbamoyl]-ethylcarbamoyl}-pyridin-2-ylmethyl)-amino]-ethyl}-carbamic acid benzyl ester (119829-32-2)

Guidance literature:

Multi-step reaction with 7 steps

1: 94 percent

2: trifluoroacetic acid / CH₂Cl₂

4: trifluoroacetic acid / CH₂Cl₂

6: trifluoroacetic acid / CH₂Cl₂

7: 40 percent / dicyclohexylcarbodiimide, 1-hydroxybenzotriazole

With benzotriazol-1-ol; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane;

DOI:10.1246/cl.1989.51

upstream raw materials:

4-Amino-N-(3-{3-[3-(7-oxo-7H-furo[3,2-g]chromen-9-yloxy)-propylcarbamoyl]-propylcarbamoyl}-propyl)-butyramide

2-[(6-{[Benzyloxycarbonyl-(2-benzyloxycarbonylamino-ethyl)-amino]-methyl}-pyridine-2-carbonyl)-amino]-3-(3H-imidazol-4-yl)-propionic acid

8-hydroxypsoralen

9-(3-Amino-propoxy)-furo[3,2-g]chromen-7-one

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