(p-methoxyphenyl)-1-homoisochroman

Base Information

Chemical Name:(p-methoxyphenyl)-1-homoisochroman
CAS No.:117266-89-4
Molecular Formula:C₁₇H₁₈O₂
Molecular Weight:254.329
Hs Code.:

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Chemical Property of (p-methoxyphenyl)-1-homoisochroman

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Technology Process of (p-methoxyphenyl)-1-homoisochroman

There total 5 articles about (p-methoxyphenyl)-1-homoisochroman which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 110690-19-2
2-(p-methoxyphenylhydroxymethyl)phenylpropanol

: 117266-89-4
(p-methoxyphenyl)-1-homoisochroman

Guidance literature:: With potassium hydrogencarbonate; for 1h; Heating;

Reference yield:

: 104-92-7
1-bromo-4-methoxy-benzene

: 117266-89-4
(p-methoxyphenyl)-1-homoisochroman

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) Mg

2: sodium dichromate, conc. H₂SO₄, sodium benzosulfonate / H₂O / 4.5 h / 50 - 55 °C

3: 90 percent / LiAlH₄ / diethyl ether

4: 90 percent / potassium hydrogencarbonate / 1 h / Heating

With lithium aluminium tetrahydride; sodium dichromate; sulfuric acid; sodium phenylsulfonate; potassium hydrogencarbonate; magnesium; In diethyl ether; water;

Reference yield:

: 79560-27-3
1-hydroxy-1-(4-methoxyphenyl)tetralin

: 117266-89-4
(p-methoxyphenyl)-1-homoisochroman

Guidance literature:: Multi-step reaction with 3 steps

1: sodium dichromate, conc. H₂SO₄, sodium benzosulfonate / H₂O / 4.5 h / 50 - 55 °C

2: 90 percent / LiAlH₄ / diethyl ether

3: 90 percent / potassium hydrogencarbonate / 1 h / Heating

With lithium aluminium tetrahydride; sodium dichromate; sulfuric acid; sodium phenylsulfonate; potassium hydrogencarbonate; In diethyl ether; water;