C₂₇H₃₃N₃O₆*C₂HF₃O₂

Base Information

Chemical Name:C₂₇H₃₃N₃O₆*C₂HF₃O₂
CAS No.:1570068-91-5
Molecular Formula:C₂HF₃O₂*C₂₇H₃₃N₃O₆
Molecular Weight:609.599
Hs Code.:

C<sub>27</sub>H<sub>33</sub>N<sub>3</sub>O<sub>6</sub>*C<sub>2</sub>HF<sub>3</sub>O<sub>2</sub>

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Chemical Property of C₂₇H₃₃N₃O₆*C₂HF₃O₂

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Technology Process of C₂₇H₃₃N₃O₆*C₂HF₃O₂

There total 6 articles about C₂₇H₃₃N₃O₆*C₂HF₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₇H₃₁N₃O₆

: 76-05-1
trifluoroacetic acid

: 1570068-93-7
C₂₇H₃₃N₃O₆*C₂HF₃O₂

: 1570068-91-5
C₂₇H₃₃N₃O₆*C₂HF₃O₂

Guidance literature:: C₂₇H₃₁N₃O₆; With sodium cyanoborohydride; In methanol; N,N-dimethyl-formamide; at 20 ℃; for 16h; Inert atmosphere;

trifluoroacetic acid; In water; acetonitrile; Overall yield = 4.2 mg; Optical yield = 56 %de;
DOI:10.1021/ol5003797

Reference yield:

: C₁₂H₁₅NO₃

: 1570068-93-7
C₂₇H₃₃N₃O₆*C₂HF₃O₂

: 1570068-91-5
C₂₇H₃₃N₃O₆*C₂HF₃O₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: 6-chloro-3-((dimethylamino)(dimethyliminio)methyl)-1H-benzo[d][1,2,3]triazol-3-ium-1-olatehexafluorophosphate(V); 2,6-dimethylpyridine / dichloromethane; N,N-dimethyl-formamide / 0.08 h / 0 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: hydrogenchloride / 1,4-dioxane / 3 h / 0 - 20 °C / Inert atmosphere

3.1: acetic acid / N,N-dimethyl-formamide / 1.5 h / 20 °C / Inert atmosphere

4.1: sodium cyanoborohydride / N,N-dimethyl-formamide; methanol / 16 h / 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; hydrogenchloride; 6-chloro-3-((dimethylamino)(dimethyliminio)methyl)-1H-benzo[d][1,2,3]triazol-3-ium-1-olatehexafluorophosphate(V); sodium cyanoborohydride; acetic acid; In 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol5003797

Reference yield:

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 1570068-93-7
C₂₇H₃₃N₃O₆*C₂HF₃O₂

: 1570068-91-5
C₂₇H₃₃N₃O₆*C₂HF₃O₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 0.08 h / 0 °C / Inert atmosphere

1.2: 16 h / 0 - 20 °C / Inert atmosphere

2.1: hydrogenchloride / 1,4-dioxane / 0 - 20 °C / Inert atmosphere

3.1: 6-chloro-3-((dimethylamino)(dimethyliminio)methyl)-1H-benzo[d][1,2,3]triazol-3-ium-1-olatehexafluorophosphate(V); 2,6-dimethylpyridine / dichloromethane; N,N-dimethyl-formamide / 0.08 h / 0 °C / Inert atmosphere

3.2: 0 - 20 °C / Inert atmosphere

4.1: hydrogenchloride / 1,4-dioxane / 3 h / 0 - 20 °C / Inert atmosphere

5.1: acetic acid / N,N-dimethyl-formamide / 1.5 h / 20 °C / Inert atmosphere

6.1: sodium cyanoborohydride / N,N-dimethyl-formamide; methanol / 16 h / 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; hydrogenchloride; dmap; 6-chloro-3-((dimethylamino)(dimethyliminio)methyl)-1H-benzo[d][1,2,3]triazol-3-ium-1-olatehexafluorophosphate(V); sodium cyanoborohydride; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol5003797