CF₃CCCF₃Ni{As(CH₃)2C₆H₅}2

Base Information

Chemical Name:CF₃CCCF₃Ni{As(CH₃)2C₆H₅}2
CAS No.:52544-45-3
Molecular Formula:C₂₀H₂₂As₂F₆Ni
Molecular Weight:584.918
Hs Code.:

CF<sub>3</sub>CCCF<sub>3</sub>Ni{As(CH<sub>3</sub>)2C<sub>6</sub>H<sub>5</sub>}2

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Suppliers and Price of CF₃CCCF₃Ni{As(CH₃)2C₆H₅}2

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of CF₃CCCF₃Ni{As(CH₃)2C₆H₅}2

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Technology Process of CF₃CCCF₃Ni{As(CH₃)2C₆H₅}2

There total 2 articles about CF₃CCCF₃Ni{As(CH₃)2C₆H₅}2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 548757-70-6,33154-75-5,12126-69-1,548757-71-7,39330-67-1
[Ni(1,5,9-cyclododecatriene)]

: 696-26-4
dimethylphenylarsine

: 692-50-2
hexafluoro-2-butyne

: 52544-45-3
CF₃CCCF₃Ni{As(CH₃)2C₆H₅}2

Guidance literature:: In diethyl ether; react. in ether at -78 °C (4 h), then addn. of As(CH3)2C6H5 in toluene at equal temp., warming to room temp., concg. in vac.;; crystn.;

Reference yield:

: (trans,trans,trans-1,5,9-cyclododecatriene)nickel

: 696-26-4
dimethylphenylarsine

: 692-50-2
hexafluoro-2-butyne

: 52544-45-3
CF₃CCCF₃Ni{As(CH₃)2C₆H₅}2

Guidance literature:: In diethyl ether; CF3CCCF3 in excess; between -196 and -78°C; connected adding of As(CH3)2C6H5 in toluene to the mixture;
DOI:10.1039/DT9740000097