1-tert-butyl-3-phenyl-4,5-dihydro-1H-imidazol-3-ium chloride

Base Information

Chemical Name:1-tert-butyl-3-phenyl-4,5-dihydro-1H-imidazol-3-ium chloride
CAS No.:1185252-18-9
Molecular Formula:C₁₃H₁₉N₂*Cl
Molecular Weight:238.76
Hs Code.:

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Chemical Property of 1-tert-butyl-3-phenyl-4,5-dihydro-1H-imidazol-3-ium chloride

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Technology Process of 1-tert-butyl-3-phenyl-4,5-dihydro-1H-imidazol-3-ium chloride

There total 1 articles about 1-tert-butyl-3-phenyl-4,5-dihydro-1H-imidazol-3-ium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 64469-34-7
N¹-tert.-Butyl-N²-phenylethylendiamin

: 122-51-0
orthoformic acid triethyl ester

: 1185252-18-9
1-tert-butyl-3-phenyl-4,5-dihydro-1H-imidazol-3-ium chloride

Guidance literature:: With hydrogenchloride; formic acid; In water; at 120 ℃; for 12h; Inert atmosphere;
DOI:10.1039/b818091a

Reference yield: 32.0%

: 52462-29-0
[ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂

: 1185252-18-9
1-tert-butyl-3-phenyl-4,5-dihydro-1H-imidazol-3-ium chloride

: 7681-82-5,24359-64-6,41927-88-2,115813-40-6
sodium iodide

: ((CH₃C₆H₄CH(CH₃)2)RuI(CH₂(CH₃)2CNC₃H₄NC₆H₅))

Guidance literature:: With n-BuLi; In tetrahydrofuran; mixt. imidazolium salt and n-BuLi in THF was stirred at 0°C for 5h, Ru complex and NaI were added, react. mixt. was stirred at room temp . overnight; solvents were removed in vacuo, residue was extd. with CH2Cl2 and filtered through Celite, solvent was removed in vacuo, residue was recrystd. from hexane-CH2Cl2;
DOI:10.1039/b818091a