Mo(η6-PhPEt2)(PPh2CH2CH2PPh2)(PEt2Ph)

Base Information

Chemical Name:Mo(η6-PhPEt2)(PPh2CH2CH2PPh2)(PEt2Ph)
CAS No.:98703-53-8
Molecular Formula:C₄₆H₅₄MoP₄
Molecular Weight:826.77
Hs Code.:

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Chemical Property of Mo(η6-PhPEt2)(PPh2CH2CH2PPh2)(PEt2Ph)

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Technology Process of Mo(η6-PhPEt2)(PPh2CH2CH2PPh2)(PEt2Ph)

There total 1 articles about Mo(η6-PhPEt2)(PPh2CH2CH2PPh2)(PEt2Ph) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 40219-67-8
MoCl₄(dppe)

: 1605-53-4
diethyl-phenyl-phosphine

: 98703-53-8
Mo(η6-PhPEt2)(PPh2CH2CH2PPh2)(PEt2Ph)

Guidance literature:: With magnesium; In tetrahydrofuran; MoCl4(DPPE) dissolved under Ar in soln. of PEt2Ph in degassed THF, treated with excess Mg; filtered through Celite under Ar, concd., pptd. with degassed MeOH, recrystd. from C6H6/MeOH, dried under vac.; elem. anal.;
DOI:10.1016/0022-328X(85)87215-6

Reference yield:

: 56613-96-8,77210-60-7,15584-93-7,19187-82-7
bis(acetonitrile)tetrachloromolybdenum(IV)

: 98703-53-8
Mo(η6-PhPEt2)(PPh2CH2CH2PPh2)(PEt2Ph)

: 109214-64-4,59752-91-9
Mo₂Cl₄(P(C₂H₅)2(C₆H₅))4

Guidance literature:: In tetrahydrofuran; equimolar mixt. of Mo(η6-PhPEt2)(PPh2CH2CH2PPh2)(PEt2Ph) and MoCl4(CH3CN) in THF was stirred for 1 h; evapd. to dryness, the residue was dissolved in C6H6; detected by (31)P NMR;