Technology Process of 2-Cyclohexene-1-acetamide, N-methyl-N-phenyl-
There total 5 articles about 2-Cyclohexene-1-acetamide, N-methyl-N-phenyl- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: Thionyl chloride / 3 h / Heating
2: 0 °C
3: 1) sodium hydride / 1) THF, room temp. until the evolution of H2 ceased. 2) room temp., overnight
4: 25 percent Chromat. / tetrakis(triphenylphosphine)nickel(0), triethylaluminum / tetrahydrofuran; toluene / 5 h / 120 °C
With
thionyl chloride; tetrakis(triphenylphosphine)nickel(0); triethylaluminum; sodium hydride;
In
tetrahydrofuran; toluene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 0 °C
2: 1) sodium hydride / 1) THF, room temp. until the evolution of H2 ceased. 2) room temp., overnight
3: 25 percent Chromat. / tetrakis(triphenylphosphine)nickel(0), triethylaluminum / tetrahydrofuran; toluene / 5 h / 120 °C
With
tetrakis(triphenylphosphine)nickel(0); triethylaluminum; sodium hydride;
In
tetrahydrofuran; toluene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1) sodium hydride / 1) THF, room temp. until the evolution of H2 ceased. 2) room temp., overnight
2: 25 percent Chromat. / tetrakis(triphenylphosphine)nickel(0), triethylaluminum / tetrahydrofuran; toluene / 5 h / 120 °C
With
tetrakis(triphenylphosphine)nickel(0); triethylaluminum; sodium hydride;
In
tetrahydrofuran; toluene;