C₄₅H₄₉F₅N₆O₁₀

Base Information

Chemical Name:C₄₅H₄₉F₅N₆O₁₀
CAS No.:193354-23-3
Molecular Formula:C₄₅H₄₉F₅N₆O₁₀
Molecular Weight:928.91
Hs Code.:

C<sub>45</sub>H<sub>49</sub>F<sub>5</sub>N<sub>6</sub>O<sub>10</sub>

Synonyms:

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Chemical Property of C₄₅H₄₉F₅N₆O₁₀

Chemical Property:

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Technology Process of C₄₅H₄₉F₅N₆O₁₀

There total 13 articles about C₄₅H₄₉F₅N₆O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 71655-17-9
(E)-3-hexen-1,6-diol

: 193354-23-3
C₄₅H₄₉F₅N₆O₁₀

Guidance literature:: Multi-step reaction with 18 steps

1: 18.74 g / DMAP, Et₃N / CH₂Cl₂ / Ambient temperature

2: 13.90 g / AD-mix-β, MeSO2NH2 / 2-methyl-propan-2-ol; H2O / 10 h / 0 °C

3: Amberlyst 15 / 4 h

4: 4.32 g / K₂CO₃ / methanol; H₂O / Ambient temperature

5: 93 percent / CBr₄, PPh₃ / CH₂Cl₂ / 1 h / Ambient temperature

6: 73 percent / toluene / 60 h

7: 100 percent / HCl / H₂O; tetrahydrofuran / 0.5 h

8: H₂ / Pd/C / methanol / 0.5 h

9: 1.97 g / Et₃N / methanol / 2 h / Ambient temperature

10: Et₃N / CH₂Cl₂ / 2 h / Ambient temperature

11: 3.71 g / NaN₃ / dimethylformamide / 20 h / 85 - 90 °C

12: 100 percent / H₂ / Pd/C / methanol / 8 h

13: 41 percent / CH₂Cl₂; triethylamine / 8 h / Ambient temperature

14: 100 percent / i-Pr₂NEt / tetrahydrofuran / Ambient temperature

15: H₂ / Pd/C / methanol / 3 h

16: 78 percent / i-Pr₂NEt / tetrahydrofuran / Ambient temperature

17: NaOH / tetrahydrofuran; methanol / 4 h / Ambient temperature

18: 79 mg / pyridine; dimethylformamide / 4 h / Ambient temperature

With hydrogenchloride; dmap; sodium hydroxide; sodium azide; Amberlyst 15; carbon tetrabromide; methanesulfonamide; AD-mix-β; hydrogen; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; palladium on activated charcoal; In tetrahydrofuran; pyridine; methanol; dichloromethane; water; triethylamine; N,N-dimethyl-formamide; toluene; tert-butyl alcohol;
DOI:10.1016/S0040-4020(97)90388-4

Reference yield:

: 116701-54-3
(4R,5R)-(+)-4,5-bis(2-bromoethyl)-2,2-dimethyl-1,3-dioxolane

: 193354-23-3
C₄₅H₄₉F₅N₆O₁₀

Guidance literature:: Multi-step reaction with 13 steps

1: 73 percent / toluene / 60 h

2: 100 percent / HCl / H₂O; tetrahydrofuran / 0.5 h

3: H₂ / Pd/C / methanol / 0.5 h

4: 1.97 g / Et₃N / methanol / 2 h / Ambient temperature

5: Et₃N / CH₂Cl₂ / 2 h / Ambient temperature

6: 3.71 g / NaN₃ / dimethylformamide / 20 h / 85 - 90 °C

7: 100 percent / H₂ / Pd/C / methanol / 8 h

8: 41 percent / CH₂Cl₂; triethylamine / 8 h / Ambient temperature

9: 100 percent / i-Pr₂NEt / tetrahydrofuran / Ambient temperature

10: H₂ / Pd/C / methanol / 3 h

11: 78 percent / i-Pr₂NEt / tetrahydrofuran / Ambient temperature

12: NaOH / tetrahydrofuran; methanol / 4 h / Ambient temperature

13: 79 mg / pyridine; dimethylformamide / 4 h / Ambient temperature

With hydrogenchloride; sodium hydroxide; sodium azide; hydrogen; triethylamine; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In tetrahydrofuran; pyridine; methanol; dichloromethane; water; triethylamine; N,N-dimethyl-formamide; toluene;
DOI:10.1016/S0040-4020(97)90388-4

Reference yield:

: 165195-72-2
(4R,5R)-4,5-Dihydroxy-azepane-1-carboxylic acid tert-butyl ester

: 193354-23-3
C₄₅H₄₉F₅N₆O₁₀

Guidance literature:: Multi-step reaction with 9 steps

1: Et₃N / CH₂Cl₂ / 2 h / Ambient temperature

2: 3.71 g / NaN₃ / dimethylformamide / 20 h / 85 - 90 °C

3: 100 percent / H₂ / Pd/C / methanol / 8 h

4: 41 percent / CH₂Cl₂; triethylamine / 8 h / Ambient temperature

5: 100 percent / i-Pr₂NEt / tetrahydrofuran / Ambient temperature

6: H₂ / Pd/C / methanol / 3 h

7: 78 percent / i-Pr₂NEt / tetrahydrofuran / Ambient temperature

8: NaOH / tetrahydrofuran; methanol / 4 h / Ambient temperature

9: 79 mg / pyridine; dimethylformamide / 4 h / Ambient temperature

With sodium hydroxide; sodium azide; hydrogen; triethylamine; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In tetrahydrofuran; pyridine; methanol; dichloromethane; triethylamine; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(97)90388-4