5-(1-butenyl)-6,8-dimethyl-1-phenylsulfonyl-1,6,7,8-tetrahydrocyclopentindole

Base Information

• Chemical Name: 5-(1-butenyl)-6,8-dimethyl-1-phenylsulfonyl-1,6,7,8-tetrahydrocyclopentindole
• CAS No.: 132142-88-2
• Molecular Formula: C₂₃H₂₅NO₂S
• Molecular Weight: 379.523

Synonyms:

Chemical Property of 5-(1-butenyl)-6,8-dimethyl-1-phenylsulfonyl-1,6,7,8-tetrahydrocyclopentindole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5-(1-butenyl)-6,8-dimethyl-1-phenylsulfonyl-1,6,7,8-tetrahydrocyclopentindole

There total 2 articles about 5-(1-butenyl)-6,8-dimethyl-1-phenylsulfonyl-1,6,7,8-tetrahydrocyclopentindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

5-(3-butenyl)-6,8-dimethyl-1-phenylsulfonyl-1,6,7,8-tetrahydrocyclopentindole (132142-87-1,132142-93-9) → 5-(1-butenyl)-6,8-dimethyl-1-phenylsulfonyl-1,6,7,8-tetrahydrocyclopentindole (132142-88-2,132202-19-8)

Guidance literature:

rhodium(III) chloride; In ethanol; at 100 ℃; for 50h; sealed tube;

DOI:10.1016/S0040-4020(01)86755-7

Reference yield:

2-[(2R,3R)-2-(1-Benzenesulfonyl-1H-pyrrol-2-yl)-1-hydroxy-3,5-dimethyl-cyclopentyl]-hex-5-enal (132142-86-0) → 5-(1-butenyl)-6,8-dimethyl-1-phenylsulfonyl-1,6,7,8-tetrahydrocyclopentindole (132142-88-2,132202-19-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 6percent H₂SO₄ / propan-2-ol / 1 h / Heating

2: 80 percent / RhCl₃*3H₂O / ethanol / 50 h / 100 °C / sealed tube

With sulfuric acid; rhodium(III) chloride; In ethanol; isopropyl alcohol;

DOI:10.1016/S0040-4020(01)86755-7

Reference yield: 50.0%

5-(1-butenyl)-6,8-dimethyl-1-phenylsulfonyl-1,6,7,8-tetrahydrocyclopentindole (132142-88-2,132202-19-8) → (+/-)-trans-trikentrin (107368-93-4,107438-54-0,127515-90-6,127592-48-7,132295-93-3) + (+/-)-cis-trikentrin B (107368-93-4,107438-54-0,127515-90-6,127592-48-7,132295-93-3)

Guidance literature:

With potassium hydroxide; In methanol; 1,2-dimethoxyethane; water; for 3h; Heating;

DOI:10.1016/S0040-4020(01)86755-7

upstream raw materials:

5-(3-butenyl)-6,8-dimethyl-1-phenylsulfonyl-1,6,7,8-tetrahydrocyclopentindole

2-[(2R,3R)-2-(1-Benzenesulfonyl-1H-pyrrol-2-yl)-1-hydroxy-3,5-dimethyl-cyclopentyl]-hex-5-enal

Downstream raw materials:

(+/-)-trans-trikentrin

(+/-)-cis-trikentrin B

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 132142-88-2 5-(1-butenyl)-6,8-dimethyl-1-phenylsulfonyl-1,6,7,8-tetrahydrocyclopentindole

Send

Send

Metric Ton KG G Pound L ML

Send

Send