2-(trimethylsilyl)ethyl 2,3,6-tri-O-benzyl-4-O-<2,4,6-tri-O-benzyl-3-O-(2,4-dideoxy-2-phthalimido-β-D-xylo-hexopyranosyl)-α-D-galactopyranosyl>-β-D-galactopyranoside

Base Information

Chemical Name:2-(trimethylsilyl)ethyl 2,3,6-tri-O-benzyl-4-O-<2,4,6-tri-O-benzyl-3-O-(2,4-dideoxy-2-phthalimido-β-D-xylo-hexopyranosyl)-α-D-galactopyranosyl>-β-D-galactopyranoside
CAS No.:157553-87-2
Molecular Formula:C₇₃H₈₃NO₁₆Si
Molecular Weight:1258.54
Hs Code.:

2-(trimethylsilyl)ethyl 2,3,6-tri-O-benzyl-4-O-<2,4,6-tri-O-benzyl-3-O-(2,4-dideoxy-2-phthalimido-β-D-xylo-hexopyranosyl)-α-D-galactopyranosyl>-β-D-galactopyranoside

Synonyms:

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Chemical Property of 2-(trimethylsilyl)ethyl 2,3,6-tri-O-benzyl-4-O-<2,4,6-tri-O-benzyl-3-O-(2,4-dideoxy-2-phthalimido-β-D-xylo-hexopyranosyl)-α-D-galactopyranosyl>-β-D-galactopyranoside

Chemical Property:

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Technology Process of 2-(trimethylsilyl)ethyl 2,3,6-tri-O-benzyl-4-O-<2,4,6-tri-O-benzyl-3-O-(2,4-dideoxy-2-phthalimido-β-D-xylo-hexopyranosyl)-α-D-galactopyranosyl>-β-D-galactopyranoside

There total 1 articles about 2-(trimethylsilyl)ethyl 2,3,6-tri-O-benzyl-4-O-<2,4,6-tri-O-benzyl-3-O-(2,4-dideoxy-2-phthalimido-β-D-xylo-hexopyranosyl)-α-D-galactopyranosyl>-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₈₇H₉₁NO₁₈Si

: 157553-87-2
2-(trimethylsilyl)ethyl 2,3,6-tri-O-benzyl-4-O-<2,4,6-tri-O-benzyl-3-O-(2,4-dideoxy-2-phthalimido-β-D-xylo-hexopyranosyl)-α-D-galactopyranosyl>-β-D-galactopyranoside

Guidance literature:: With sodium methylate; In methanol; Yield given;
DOI:10.3891/acta.chem.scand.48-0356

Reference yield:

: 157553-87-2
2-(trimethylsilyl)ethyl 2,3,6-tri-O-benzyl-4-O-<2,4,6-tri-O-benzyl-3-O-(2,4-dideoxy-2-phthalimido-β-D-xylo-hexopyranosyl)-α-D-galactopyranosyl>-β-D-galactopyranoside

: 157553-88-3
2-(trimethylsilyl)ethyl 4-O-<3-O-(2,4-dideoxy-2-acetamido-β-D-xylo-hexopyranosyl)-α-D-galactopyranosyl>-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / 10percent Pd/C / acetic acid / 1.5 h

2: hydrazine hydrate / ethanol / 2 h / Heating

3: methanol; H₂O / 1 h

With hydrogen; hydrazine hydrate; palladium on activated charcoal; In methanol; ethanol; water; acetic acid;
DOI:10.3891/acta.chem.scand.48-0356