<2R^*-<2α(S^*),3β,11bβ>>-10-benzyloxy-2-<(6-benzyloxy-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-yl)methyl>-3-ethyl-1,3,4,6,7,11b-hexahydro-9-methoxy-2H-benzoquinolizine

Base Information

• Chemical Name: <2R^*-<2α(S^*),3β,11bβ>>-10-benzyloxy-2-<(6-benzyloxy-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-yl)methyl>-3-ethyl-1,3,4,6,7,11b-hexahydro-9-methoxy-2H-benzo
• Molecular Formula: C₄₂H₄₇N₃O₃
• Molecular Weight: 641.853

Synonyms:

Chemical Property of <2R^*-<2α(S^*),3β,11bβ>>-10-benzyloxy-2-<(6-benzyloxy-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-yl)methyl>-3-ethyl-1,3,4,6,7,11b-hexahydro-9-methoxy-2H-benzo

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

There total 8 articles about <2R^*-<2α(S^*),3β,11bβ>>-10-benzyloxy-2-<(6-benzyloxy-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-yl)methyl>-3-ethyl-1,3,4,6,7,11b-hexahydro-9-methoxy-2H-benzoquinolizine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

(+/-)-10-benzyloxy-2β-<(6-benzyloxy-4,9-dihydro-3H-pyrido<3,4-b>indol-1-yl)methyl>-3α-ethyl-1,3,4,6,7,11bα-hexahydro-9-methoxy-2H-benzoquinolizine (75029-27-5) → <2R*-<2α(R*),3β,11bβ>>-10-benzyloxy-2-<(6-benzyloxy-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-yl)methyl>-3-ethyl-1,3,4,6,7,11b-hexahydro-9-methoxy-2H-benzoquinolizine (75029-28-6,75045-62-4) + <2R*-<2α(S*),3β,11bβ>>-10-benzyloxy-2-<(6-benzyloxy-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-yl)methyl>-3-ethyl-1,3,4,6,7,11b-hexahydro-9-methoxy-2H-benzoquinolizine (75029-28-6,75045-62-4)

Guidance literature:

With hydrogen; platinum(IV) oxide; In 1,4-dioxane; at 19 ℃; for 1.5h;

Reference yield: 54.0%

(+/-)-10-benzyloxy-2β-<(6-benzyloxy-4,9-dihydro-3H-pyrido<3,4-b>indol-1-yl)methyl>-3α-ethyl-1,3,4,6,7,11bα-hexahydro-9-methoxy-2H-benzoquinolizine (75029-27-5) → <2R*-<2α(R*),3β,11bβ>>-10-benzyloxy-2-<(6-benzyloxy-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-yl)methyl>-3-ethyl-1,3,4,6,7,11b-hexahydro-9-methoxy-2H-benzoquinolizine (75029-28-6,75045-62-4) + <2R*-<2α(S*),3β,11bβ>>-10-benzyloxy-2-<(6-benzyloxy-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-yl)methyl>-3-ethyl-1,3,4,6,7,11b-hexahydro-9-methoxy-2H-benzoquinolizine (75029-28-6,75045-62-4)

Guidance literature:

With hydrogen; platinum(IV) oxide; In 1,4-dioxane; at 19 ℃; for 1.5h;

Reference yield:

(+/-)-10-benzyloxy-3α-ethyl-1,3,4,6,7,11bα-hexahydro-9-methoxy-2H-benzoquinolizine-2β-acetic acid (73053-59-5,82536-15-0) → <2R*-<2α(R*),3β,11bβ>>-10-benzyloxy-2-<(6-benzyloxy-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-yl)methyl>-3-ethyl-1,3,4,6,7,11b-hexahydro-9-methoxy-2H-benzoquinolizine (75029-28-6,75045-62-4)

Guidance literature:

Multi-step reaction with 3 steps

1: 96 percent / (C₂H₅)3N, diethyl phosphorocyanidate / dimethylformamide / 6 h / Ambient temperature

2: 59 percent / POCl₃ / toluene / 2.5 h / Heating

3: 54 percent / H₂ / PtO₂ / dioxane / 1.5 h / 19 °C / 760 Torr

With diethyl cyanophosphonate; hydrogen; triethylamine; trichlorophosphate; platinum(IV) oxide; In 1,4-dioxane; N,N-dimethyl-formamide; toluene;

upstream raw materials:

(+/-)-10-benzyloxy-2β-<(6-benzyloxy-4,9-dihydro-3H-pyrido<3,4-b>indol-1-yl)methyl>-3α-ethyl-1,3,4,6,7,11bα-hexahydro-9-methoxy-2H-benzoquinolizine

5-benzyloxytryptamine

(+/-)-10-benzyloxy-N-<2-(5-benzyloxy-1H-indol-3-yl)ethyl>-3α-ethyl-1,3,4,6,7,11bα-hexahydro-9-methoxy-2H-benzoquinolizine-2β-acetamide

(+/-)-10-benzyloxy-3α-ethyl-1,3,4,6,7,11bα-hexahydro-9-methoxy-2H-benzoquinolizine-2β-acetic acid

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 75029-28-6 <2R^*-<2α(S^*),3β,11bβ>>-10-benzyloxy-2-<(6-benzyloxy-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-yl)methyl>-3-ethyl-1,3,4,6,7,11b-hexahydro-9-methoxy-2H-benzoquinolizine

Send

Send

Metric Ton KG G Pound L ML

Send

Send