chromium⁽⁰⁾ hexakis(phenyl isocyanide)

Base Information

Chemical Name:chromium⁽⁰⁾ hexakis(phenyl isocyanide)
CAS No.:17375-15-4
Molecular Formula:C₄₂H₃₀CrN₆
Molecular Weight:670.736
Hs Code.:

chromium<sup>(0)</sup> hexakis(phenyl isocyanide)

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Chemical Property of chromium⁽⁰⁾ hexakis(phenyl isocyanide)

Chemical Property:

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Technology Process of chromium⁽⁰⁾ hexakis(phenyl isocyanide)

There total 5 articles about chromium⁽⁰⁾ hexakis(phenyl isocyanide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

: chromium chloride hexahydrate

: 1197040-29-1,931-54-4
phenyl isocyanate

: 17375-15-4
chromium⁽⁰⁾ hexakis(phenyl isocyanide)

Guidance literature:: With t-butylamine or isopropyl amine or PEt₂Ph; Zn#Hg; In ethanol; (N2); chromium(II) soln. (prepd. from CrCl3*6H2O/EtOH and Zn#Hg) syringed into stirred mixt. of C6H5NC and t-butylamine in EtOH, stirred for 30min at room temp.; solid filtered, extd. (C6H6), concd.;
DOI:10.1016/S0022-328X(00)98713-8

Reference yield:

: bis(η5-2,4-dimethylpentadienyl)chromium

: 1197040-29-1,931-54-4
phenyl isocyanate

: 17375-15-4
chromium⁽⁰⁾ hexakis(phenyl isocyanide)

Guidance literature:: In tetrahydrofuran; N2 atmosphere; adn. of C6H5NC to a soln. of the Cr complex in THF at -78°C; soln. was allowed to warm to room temp. for 12 h;; evapn.; extd. with hexane for several times; the combined extracts were filtered and concd.; crystn. on cooling;;
DOI:10.1021/om00154a026

Reference yield:

: 14404-41-2,92141-39-4
chromium(II) acetate

: 1197040-29-1,931-54-4
phenyl isocyanate

: 17375-15-4
chromium⁽⁰⁾ hexakis(phenyl isocyanide)

Guidance literature:: In methanol; reaction of Cr(II)-acetate with C6H5NC in methanol (mole ratio of educts 3 : 18);; pptn., washing with acetic acid and alc., then with pure alc.;;