(-)-3-carbo(-)menthoxy-r-9,c-11,c-13,c-15-tetrahexyl-7,17:8,16-dimetheno-9H,11H,13H,15H-quinoxalino<2''',3''':2''',3'''><1,4>benzodioxonino<10''',9''':5,6>quinoxalino<2',3':2',3'>quinoxalino<2'',3'':2'',3''><1,4>dioxonino<6'',5'':9',10'><1,4>benzodio...

Base Information

• Chemical Name: (-)-3-carbo(-)menthoxy-r-9,c-11,c-13,c-15-tetrahexyl-7,17:8,16-dimetheno-9H,11H,13H,15H-quinoxalino<2''',3''':2''',3'''><1,4>benzodioxonino<10''',9''':5,6>quinoxalino<2',3':2',3'>quinoxalino<2'',3'':2'',3''><1,4>dioxonino<6'',5'':9',10'><1,4>benzodio...
• CAS No.: 124381-15-3
• Molecular Formula: C₉₅H₉₈N₈O₁₀
• Molecular Weight: 1511.87

Synonyms:

Chemical Property of (-)-3-carbo(-)menthoxy-r-9,c-11,c-13,c-15-tetrahexyl-7,17:8,16-dimetheno-9H,11H,13H,15H-quinoxalino<2''',3''':2''',3'''><1,4>benzodioxonino<10''',9''':5,6>quinoxalino<2',3':2',3'>quinoxalino<2'',3'':2'',3''><1,4>dioxonino<6'',5'':9',10'><1,4>benzodio...

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Technology Process of (-)-3-carbo(-)menthoxy-r-9,c-11,c-13,c-15-tetrahexyl-7,17:8,16-dimetheno-9H,11H,13H,15H-quinoxalino<2''',3''':2''',3'''><1,4>benzodioxonino<10''',9''':5,6>quinoxalino<2',3':2',3'>quinoxalino<2'',3'':2'',3''><1,4>dioxonino<6'',5'':9',10'><1,4>benzodio...

There total 8 articles about (-)-3-carbo(-)menthoxy-r-9,c-11,c-13,c-15-tetrahexyl-7,17:8,16-dimetheno-9H,11H,13H,15H-quinoxalino<2''',3''':2''',3'''><1,4>benzodioxonino<10''',9''':5,6>quinoxalino<2',3':2',3'>quinoxalino<2'',3'':2'',3''><1,4>dioxonino<6'',5'':9',10'><1,4>benzodio... which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

r-11,c-13,c-15,c-40-tetrahexyl-9,17-methano-11H,13H,15H-bisbenzo<5',6'>quinoxalino<2'',3'':2',3'><1,4>benzodioxonino<10',9':5,6:9'',10'':8,9><1,4>dioxonino<2,3-b>quinoxaline-8,18-diol (124381-14-2,124440-37-5) + 2,3-dichloro-6-quinoxalinecarboxylic acid (-)-menthyl ester (142437-62-5) → (+/-)-3-carbo(-)menthoxy-r-9,c-11,c-13,c-15-tetrahexyl-7,17:8,16-dimetheno-9H,11H,13H,15H-quinoxalino<2''',3''':2''',3'''><1,4>benzodioxonino<10''',9''':5,6>quinoxalino<2',3':2',3'>quinoxalino<2'',3'':2'',3''><1,4>dioxonino<6'',5'':9',10'><1,4>benzod... (124381-15-3,142507-46-8,142507-47-9)

Guidance literature:

With potassium carbonate; In dimethyl sulfoxide; at 50 ℃; for 24h;

DOI:10.1021/jo00043a015

Reference yield:

r-11,c-13,c-15,c-40-tetrahexyl-9,17-methano-11H,13H,15H-bisbenzo<5',6'>quinoxalino<2'',3'':2',3'><1,4>benzodioxonino<10',9':5,6:9'',10'':8,9><1,4>dioxonino<2,3-b>quinoxaline-8,18-diol (124381-14-2,124440-37-5) + 2,3-dichloro-6-quinoxalinecarboxylic acid (-)-menthyl ester (142437-62-5) → (+)-3-carbo(-)menthoxy-r-9,c-11,c-13,c-15-tetrahexyl-7,17:8,16-dimetheno-9H,11H,13H,15H-quinoxalino<2''',3''':2''',3'''><1,4>benzodioxonino<10''',9''':5,6>quinoxalino<2',3':2',3'>quinoxalino<2'',3'':2'',3''><1,4>dioxonino<6'',5'':9',10'><1,4>benzodio... (124381-15-3,142507-46-8,142507-47-9) + (-)-3-carbo(-)menthoxy-r-9,c-11,c-13,c-15-tetrahexyl-7,17:8,16-dimetheno-9H,11H,13H,15H-quinoxalino<2''',3''':2''',3'''><1,4>benzodioxonino<10''',9''':5,6>quinoxalino<2',3':2',3'>quinoxalino<2'',3'':2'',3''><1,4>dioxonino<6'',5'':9',10'><1,4>benzodio... (124381-15-3,142507-46-8,142507-47-9)

Guidance literature:

With potassium carbonate; In dimethyl sulfoxide; at 50 ℃; for 24h;

DOI:10.1021/jo00043a015

Reference yield:

r-11,c-13,c-15,c-40-tetrahexyl-9,17-methano-11H,13H,15H-bisbenzo<5',6'>quinoxalino<2'',3'':2',3'><1,4>benzodioxonino<10',9':5,6:9'',10'':8,9><1,4>dioxonino<2,3-b>quinoxaline-8,18-diol (124381-14-2,124440-37-5) + 2,3-dichloro-6-quinoxalinecarboxylic acid (-)-menthyl ester (142437-62-5) → (+)-3-carbo(-)menthoxy-r-9,c-11,c-13,c-15-tetrahexyl-7,17:8,16-dimetheno-9H,11H,13H,15H-quinoxalino<2''',3''':2''',3'''><1,4>benzodioxonino<10''',9''':5,6>quinoxalino<2',3':2',3'>quinoxalino<2'',3'':2'',3''><1,4>dioxonino<6'',5'':9',10'><1,4>benzodio... (124381-15-3,142507-46-8,142507-47-9) + (-)-3-carbo(-)menthoxy-r-9,c-11,c-13,c-15-tetrahexyl-7,17:8,16-dimetheno-9H,11H,13H,15H-quinoxalino<2''',3''':2''',3'''><1,4>benzodioxonino<10''',9''':5,6>quinoxalino<2',3':2',3'>quinoxalino<2'',3'':2'',3''><1,4>dioxonino<6'',5'':9',10'><1,4>benzodio... (124381-15-3,142507-46-8,142507-47-9)

Guidance literature:

With potassium carbonate; In dimethyl sulfoxide; at 50 ℃; for 24h;

DOI:10.1021/jo00043a015

upstream raw materials:

2,3-dichloroquinoxaline

tetra-C-hexylcalix<4>resorcinarene

2,3-dichloro-6-quinoxalinecarboxylic acid (-)-menthyl ester

r-11,c-13,c-15,c-40-tetrahexyl-9,17-methano-11H,13H,15H-bisbenzo<5',6'>quinoxalino<2'',3'':2',3'><1,4>benzodioxonino<10',9':5,6:9'',10'':8,9><1,4>dioxonino<2,3-b>quinoxaline-8,18-diol

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