C₂₇H₃₃BN₂O₇

Base Information

Chemical Name:C₂₇H₃₃BN₂O₇
CAS No.:1330780-99-8
Molecular Formula:C₂₇H₃₃BN₂O₇
Molecular Weight:508.379
Hs Code.:

C<sub>27</sub>H<sub>33</sub>BN<sub>2</sub>O<sub>7</sub>

Synonyms:

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Chemical Property of C₂₇H₃₃BN₂O₇

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Technology Process of C₂₇H₃₃BN₂O₇

There total 4 articles about C₂₇H₃₃BN₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 910819-13-5
tert-butyl N-(4-iodobenzoyl)-β-alaninate

: 1330780-97-6
C₁₃H₁₅BINO₄

: 1330780-99-8
C₂₇H₃₃BN₂O₇

Guidance literature:: C₁₃H₁₅BINO₄; With chloro-trimethyl-silane; ethylene dibromide; zinc; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; at 45 ℃; for 1.5h; Inert atmosphere;

tert-butyl N-(4-iodobenzoyl)-β-alaninate; With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; ruphos; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; at 60 ℃; for 5h; Inert atmosphere;
DOI:10.1021/ja205912y

Reference yield:

: (E)-6-methyl-2-styryl-1,3,6,2-dioxazaborocane-4,8-dione

: 1330780-99-8
C₂₇H₃₃BN₂O₇

Guidance literature:: Multi-step reaction with 5 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 12 h / 0 - 20 °C

2.1: magnesium(II) perchlorate / dichloromethane / 2.25 h / 20 °C

3.1: sodium tris(acetoxy)borohydride; acetic acid / dichloromethane / 16 h / 0 - 20 °C / Inert atmosphere

4.1: 1H-imidazole; iodine; triphenylphosphine / dichloromethane / 3.5 h / Inert atmosphere

5.1: chloro-trimethyl-silane; ethylene dibromide; zinc / tetrahydrofuran; 1-methyl-pyrrolidin-2-one / 1.5 h / 45 °C / Inert atmosphere

5.2: 5 h / 60 °C / Inert atmosphere

With 1H-imidazole; chloro-trimethyl-silane; magnesium(II) perchlorate; iodine; sodium tris(acetoxy)borohydride; acetic acid; ethylene dibromide; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; zinc; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; dichloromethane;
DOI:10.1021/ja205912y

Reference yield:

: N-methyliminodiacetyl (trans-3-phenyloxiran-2-yl)boronate

: 1330780-99-8
C₂₇H₃₃BN₂O₇

Guidance literature:: Multi-step reaction with 4 steps

1.1: magnesium(II) perchlorate / dichloromethane / 2.25 h / 20 °C

2.1: sodium tris(acetoxy)borohydride; acetic acid / dichloromethane / 16 h / 0 - 20 °C / Inert atmosphere

3.1: 1H-imidazole; iodine; triphenylphosphine / dichloromethane / 3.5 h / Inert atmosphere

4.1: chloro-trimethyl-silane; ethylene dibromide; zinc / tetrahydrofuran; 1-methyl-pyrrolidin-2-one / 1.5 h / 45 °C / Inert atmosphere

4.2: 5 h / 60 °C / Inert atmosphere

With 1H-imidazole; chloro-trimethyl-silane; magnesium(II) perchlorate; iodine; sodium tris(acetoxy)borohydride; acetic acid; ethylene dibromide; triphenylphosphine; zinc; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; dichloromethane;
DOI:10.1021/ja205912y