[U(NCS)4(CH₃(C₆H₅)2PO)4]

Base Information

• Chemical Name: [U(NCS)4(CH₃(C₆H₅)2PO)4]
• CAS No.: 90189-86-9
• Molecular Formula: C₅₆H₅₂N₄O₄P₄S₄U
• Molecular Weight: 1335.24
• Mol file: 90189-86-9.mol

Synonyms:

Chemical Property of [U(NCS)4(CH₃(C₆H₅)2PO)4]

Chemical Property:

Purity/Quality:

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Technology Process of [U(NCS)4(CH₃(C₆H₅)2PO)4]

There total 1 articles about [U(NCS)4(CH₃(C₆H₅)2PO)4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

uranium(IV) chloride (10026-10-5) + diphenyl(methyl)phosphine oxide (2129-89-7) → [U(NCS)4(CH3(C6H5)2PO)4] (90189-86-9)

Guidance literature:

With potassium thioacyanate; In tetrahydrofuran; treatment of UCl4 in THF with stoichiometric amount of KNCS; stirring for 12 h; addn. of excess of phosphine; stirring mixture for 18 h; evapn.to dryness;; washing residue with mixture of toluene and pentane (1:2); drying in vacuum for 8 h; elem. anal.;;

DOI:10.1016/0022-5088(84)90304-7

upstream raw materials:

uranium(IV) chloride

diphenyl(methyl)phosphine oxide