C₁₃H₂₃NO

Base Information

Chemical Name:C₁₃H₂₃NO
CAS No.:1426055-58-4
Molecular Formula:C₁₃H₂₃NO
Molecular Weight:209.332
Hs Code.:

Synonyms:

Suppliers and Price of C₁₃H₂₃NO

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₂₃NO

Chemical Property:

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Technology Process of C₁₃H₂₃NO

There total 5 articles about C₁₃H₂₃NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₃H₂₂O

: 1426055-58-4
C₁₃H₂₃NO

Guidance literature:: With hydroxylamine hydrochloride; sodium acetate; In methanol; at 20 ℃; for 0.25h;
DOI:10.1055/s-0032-1317693

Reference yield:

: 91975-82-5,114032-14-3
((1R,2S,5S)-2-Isopropenyl-5-methyl-cyclohexyl)-acetic acid methyl ester

: 1426055-58-4
C₁₃H₂₃NO

Guidance literature:: Multi-step reaction with 5 steps

1: lithium aluminium tetrahydride / diethyl ether / 2 h / 20 °C

2: dmap; triethylamine / dichloromethane / 1 h / 20 °C

3: potassium iodide / water; dimethyl sulfoxide / 12 h / 60 °C

4: diisobutylaluminium hydride / dichloromethane / 2 h / -78 °C

5: hydroxylamine hydrochloride; sodium acetate / methanol / 0.25 h / 20 °C

With dmap; lithium aluminium tetrahydride; hydroxylamine hydrochloride; sodium acetate; diisobutylaluminium hydride; triethylamine; potassium iodide; In methanol; diethyl ether; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1055/s-0032-1317693

Reference yield:

: 1426055-55-1
C₁₂H₂₂O

: 1426055-58-4
C₁₃H₂₃NO

Guidance literature:: Multi-step reaction with 4 steps

1: dmap; triethylamine / dichloromethane / 1 h / 20 °C

2: potassium iodide / water; dimethyl sulfoxide / 12 h / 60 °C

3: diisobutylaluminium hydride / dichloromethane / 2 h / -78 °C

4: hydroxylamine hydrochloride; sodium acetate / methanol / 0.25 h / 20 °C

With dmap; hydroxylamine hydrochloride; sodium acetate; diisobutylaluminium hydride; triethylamine; potassium iodide; In methanol; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1055/s-0032-1317693