C₄₂H₆₁NO₄Si

Base Information

Chemical Name:C₄₂H₆₁NO₄Si
CAS No.:1404379-99-2
Molecular Formula:C₄₂H₆₁NO₄Si
Molecular Weight:672.036
Hs Code.:

C<sub>42</sub>H<sub>61</sub>NO<sub>4</sub>Si

Synonyms:

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Chemical Property of C₄₂H₆₁NO₄Si

Chemical Property:

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Technology Process of C₄₂H₆₁NO₄Si

There total 24 articles about C₄₂H₆₁NO₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 646-07-1
4-Methylpentanoic acid

: 1404379-99-2
C₄₂H₆₁NO₄Si

Guidance literature:: Multi-step reaction with 13 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 °C

2.1: 1,1,3,3-Tetramethyldisiloxane / (Ph₃P)2IrCl(CO) / toluene / 2 h / 20 °C

3.1: hydroquinone / acetonitrile / 95 °C

4.1: methyl p-toluene sulfonate / water / 2 h / 110 °C

4.2: 4 h / 95 °C

5.1: hydrogen / rhodium contaminated with carbon / tetrahydrofuran / 7 h / 20 °C / 760.05 Torr

6.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 °C

7.1: diisobutylaluminium hydride / dichloromethane / 2 h / -78 °C

7.2: Cooling with ice

8.1: triphenylphosphine / dichloromethane / 0.33 h / Cooling with ice

8.2: 0.33 h / Cooling with ice

9.1: n-butyllithium / tetrahydrofuran

10.1: 1H-imidazole / N,N-dimethyl-formamide

11.1: pyridine / methanol

12.1: Iodine monochloride / dichloromethane

13.1: potassium phosphate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide; water

With pyridine; 1H-imidazole; potassium phosphate; n-butyllithium; 1,1,3,3-Tetramethyldisiloxane; hydrogen; Iodine monochloride; diisobutylaluminium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; hydroquinone; methyl p-toluene sulfonate; triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride; rhodium contaminated with carbon; (Ph₃P)2IrCl(CO); In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile;

Reference yield:

: 96556-40-0
methyl-3-(benzyloxy)-2.2-dimethylpropionate

: 1404379-99-2
C₄₂H₆₁NO₄Si

Guidance literature:: Multi-step reaction with 14 steps

1: lithium borohydride / tetrahydrofuran

2: triethylamine; pyridine-SO₃ complex / dichloromethane; dimethyl sulfoxide

3: toluene

4: sodium tetrahydroborate; methanol / cobalt(II) chloride hexahydrate / N,N-dimethyl-formamide

5: sodium hydroxide / ethanol

6: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / chloroform

7: tetrahydrofuran

8: palladium on activated charcoal / tetrahydrofuran

9: potassium tert-butylate / toluene

10: n-butyllithium / tetrahydrofuran

11: 1H-imidazole / N,N-dimethyl-formamide

12: pyridine / methanol

13: Iodine monochloride / dichloromethane

14: potassium phosphate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide; water

With pyridine; 1H-imidazole; methanol; dmap; sodium tetrahydroborate; potassium phosphate; lithium borohydride; n-butyllithium; pyridine-SO₃ complex; Iodine monochloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium hydroxide; bis-triphenylphosphine-palladium(II) chloride; cobalt(II) chloride hexahydrate; palladium on activated charcoal; potassium tert-butylate; In tetrahydrofuran; methanol; ethanol; dichloromethane; chloroform; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;

Reference yield:

: 14002-80-3
Methyl 2,2-dimethyl-3-hydroxypropionate

: 1404379-99-2
C₄₂H₆₁NO₄Si

Guidance literature:: Multi-step reaction with 15 steps

1: diethyl ether

2: lithium borohydride / tetrahydrofuran

3: triethylamine; pyridine-SO₃ complex / dichloromethane; dimethyl sulfoxide

4: toluene

5: sodium tetrahydroborate; methanol / cobalt(II) chloride hexahydrate / N,N-dimethyl-formamide

6: sodium hydroxide / ethanol

7: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / chloroform

8: tetrahydrofuran

9: palladium on activated charcoal / tetrahydrofuran

10: potassium tert-butylate / toluene

11: n-butyllithium / tetrahydrofuran

12: 1H-imidazole / N,N-dimethyl-formamide

13: pyridine / methanol

14: Iodine monochloride / dichloromethane

15: potassium phosphate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide; water

With pyridine; 1H-imidazole; methanol; dmap; sodium tetrahydroborate; potassium phosphate; lithium borohydride; n-butyllithium; pyridine-SO₃ complex; Iodine monochloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium hydroxide; bis-triphenylphosphine-palladium(II) chloride; cobalt(II) chloride hexahydrate; palladium on activated charcoal; potassium tert-butylate; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; chloroform; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;