Technology Process of C26H33NO6Si
There total 6 articles about C26H33NO6Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dipyridinium dichromate;
In
dichloromethane;
at 20 ℃;
for 16h;
Inert atmosphere;
Molecular sieve;
DOI:10.1021/jm201031f
- Guidance literature:
-
Multi-step reaction with 4 steps
1: N-ethyl-N,N-diisopropylamine / dichloromethane / 18 h / 20 °C / Inert atmosphere
2: selenium(IV) oxide / para-xylene / 5 h / Inert atmosphere; Reflux
3: tetrahydrofuran / 16 h / 0 - 20 °C / Inert atmosphere
4: dipyridinium dichromate / dichloromethane / 16 h / 20 °C / Inert atmosphere; Molecular sieve
With
selenium(IV) oxide; dipyridinium dichromate; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; dichloromethane; para-xylene;
DOI:10.1021/jm201031f
- Guidance literature:
-
Multi-step reaction with 3 steps
1: selenium(IV) oxide / para-xylene / 5 h / Inert atmosphere; Reflux
2: tetrahydrofuran / 16 h / 0 - 20 °C / Inert atmosphere
3: dipyridinium dichromate / dichloromethane / 16 h / 20 °C / Inert atmosphere; Molecular sieve
With
selenium(IV) oxide; dipyridinium dichromate;
In
tetrahydrofuran; dichloromethane; para-xylene;
DOI:10.1021/jm201031f