(trans-N,N'-dibenzylcyclam)Zr(CCPh)2

Base Information

Chemical Name:(trans-N,N'-dibenzylcyclam)Zr(CCPh)2
CAS No.:1238781-37-7
Molecular Formula:C₄₀H₄₄N₄Zr
Molecular Weight:672.04
Hs Code.:

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Chemical Property of (trans-N,N'-dibenzylcyclam)Zr(CCPh)2

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Technology Process of (trans-N,N'-dibenzylcyclam)Zr(CCPh)2

There total 2 articles about (trans-N,N'-dibenzylcyclam)Zr(CCPh)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 910803-93-9
(1,8-dibenzyl-1,4,8,11-tetraazacyclotetradecane)zirconiumdichloride

: 4440-01-1
lithium phenylacetylide

: 1238781-37-7
(trans-N,N'-dibenzylcyclam)Zr(CCPh)2

Guidance literature:: In tetrahydrofuran; under N2; soln. of PhCCLi in THF added slowly to THF suspn. of Zr compd.at room temp.; reacted for 12 h; solvent evapd.; extd. with toluene; taken to dryness; Et2O added; taken to dryness; washed with min. hexanes; elem. anal.;
DOI:10.1021/om100465d

Reference yield:

: 1242096-99-6
dimethyl(trans-N,N'-dibenzylcyclam^(2-))zirconium

: 536-74-3
phenylacetylene

: 1242097-03-5
Zr(C₂C₆H₅)(C₁₀H₂₀N₄(CH₂C₆H₅)CH₂C₆H₄)

: 1238781-37-7
(trans-N,N'-dibenzylcyclam)Zr(CCPh)2

Guidance literature:: In benzene-d6; under N2; soln. of Zr complex in C6D6 heated at 70°C for 2 h; PhCCH added; reacted at room temp. for 18 h; not isolated; detd. by (1)H NMR spectra;
DOI:10.1021/om100465d