dichlororuthenium(2+) 2-[(E)-cyclohexyldiazenyl]piperidin-1-ide 2-[(E)-cyclohexyldiazenyl]-2H-pyridin-1-ide

Base Information

• Chemical Name: dichlororuthenium(2+) 2-[(E)-cyclohexyldiazenyl]piperidin-1-ide 2-[(E)-cyclohexyldiazenyl]-2H-pyridin-1-ide
• CAS No.: 7238-19-9
• Molecular Formula: C₁₉H₃₁Br₂NO₂
• Molecular Weight: 465.269

Synonyms:Benzylamine,N,N-bis[2-(4-bromobutoxy)ethyl]- (7CI,8CI)

Chemical Property of dichlororuthenium(2+) 2-[(E)-cyclohexyldiazenyl]piperidin-1-ide 2-[(E)-cyclohexyldiazenyl]-2H-pyridin-1-ide

Chemical Property:

• Vapor Pressure: 0.00194mmHg at 25°C
• Boiling Point: 291.5°C at 760 mmHg
• Flash Point: 130.1°C

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of dichlororuthenium(2+) 2-[(E)-cyclohexyldiazenyl]piperidin-1-ide 2-[(E)-cyclohexyldiazenyl]-2H-pyridin-1-ide

There total 2 articles about dichlororuthenium(2+) 2-[(E)-cyclohexyldiazenyl]piperidin-1-ide 2-[(E)-cyclohexyldiazenyl]-2H-pyridin-1-ide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-Benzyl-bis-<2-(4-hydroxy-butyloxy)-aethyl>-amin (2159-62-8) → N-Benzyl-bis-<2-(4-brom-butyloxy)-aethyl>-amin (7238-19-9)

Guidance literature:

Multistep reaction; (i) aq. HBr, (ii) PBr₃, CHCl₃;

Reference yield:

N-benzyl-2-chloro-N-(2-chloroethyl)ethanamine hydrochloride (10429-82-0) → N-Benzyl-bis-<2-(4-brom-butyloxy)-aethyl>-amin (7238-19-9)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) Na, (ii) /BRN= 4161373/

2: (i) aq. HBr, (ii) PBr₃, CHCl₃

upstream raw materials:

N-Benzyl-bis-<2-(4-hydroxy-butyloxy)-aethyl>-amin

N-benzyl-2-chloro-N-(2-chloroethyl)ethanamine hydrochloride

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