[Ru(II)(CO)(dibenzo[f,h]quinoxaline(-1H))2(PPh₂Me)]

Base Information

• Chemical Name: [Ru(II)(CO)(dibenzo[f,h]quinoxaline(-1H))2(PPh₂Me)]
• CAS No.: 913185-35-0
• Molecular Formula: C₄₆H₃₁N₄OPRu
• Molecular Weight: 787.822

Synonyms:

Chemical Property of [Ru(II)(CO)(dibenzo[f,h]quinoxaline(-1H))2(PPh₂Me)]

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of [Ru(II)(CO)(dibenzo[f,h]quinoxaline(-1H))2(PPh₂Me)]

There total 1 articles about [Ru(II)(CO)(dibenzo[f,h]quinoxaline(-1H))2(PPh₂Me)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[Ru(II)(CO)2(dibenzo[f,h]quinoxaline(-1H))2] + diphenyl(methyl)phosphine (1486-28-8) → [Ru(II)(CO)(dibenzo[f,h]quinoxaline(-1H))2(PPh2Me)] (913185-35-0)

Guidance literature:

With Me₃NO; In further solvent(s); under N2; Ru complex in anhyd. diethyleneglycol monoethyl ether heated at 130°C (oil bath); Me3NO in the same solvent added dropwise over5 min; PPh2Me added; stirred at 160°C for 24 h; solvent evapd. under vac.; dissolved in CH2Cl2; soln. washed with distd.H2O; dried (MgSO4); evapd. to dryness; pyrified by column chromy. (sili ca gel, ethyl acetate-hexane 1:5); recrystd. from CH2Cl2-MeOH at room temp.; elem. anal.;

DOI:10.1021/ic060066g

upstream raw materials:

diphenyl(methyl)phosphine

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